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2021/11/30 (Tuesday)

Previous Day

  • Lab in-personnel: Matt, Himangshu, Giulia
Status Beginning Run 75.
1K Pot isolated. MB raised. Cryostat vacuum jacket (CVJ) pumped out.
1050 Turbo on IVC = 14 nbar. With Turbo valved out for 1 minute, IVC = 190 nbar
1050 Check fridge pressures: LHe trap/Condenser/Still = 31.3/1.3/2.0 mbar. Pump out with scroll pump.
Throughput test procedure, Cold Trap 1:
  1. All mixture in dump, LN2 trap 1 cold, condenser & still valves open (3He pump on - optional)
  2. Open V9, V13a, V12a+speedivalve, V3. Wait for G1 to be close to G2.
  3. Close V12a+speedivalve and V3, open V1
  4. monitor G1
1130 Perform mixture throughput test at MC = 300 K using above procedure with 3He pump on. Let G1 rise to 535 mbar before Step 3, then it falls to 41 mbar and starts to rise. Throughput = 5.6 mbar/min.
1140 Check pressure in 1K Pot: 22 mbar on P2, 0.03 atm on mechanical gauge. Pump out with Scroll Pump
1145 With 1K Pot speedivalve and needle valve closed, pump on Main Bath with scroll pump. Once P2 < 2 mbar, open 1K Pot speedivalve and needle valve (5 turns) to pump out 1K pot volume to < 1 mbar on P2.
1150 Close off scroll pump, then pressurize bath and 1K Pot (both sides) to about 0.5 bar with helium. Then pump it out again with scroll pump to < 1 mbar.
1200 Close off scroll pump, then pressurize bath and 1K Pot (both sides) to about 0.5 bar with helium. Then pump it out again with scroll pump to < 1 mbar.
1205 Pressurize main bath and 1K Pot (both sides) with helium to 420 mbar+1atm on G3, then close 1K Pot speedivalve and needle valve.
1325 As on 2021 June 9, we will flow mixture through the fridge during LN2 cooldown. Let mixture from dump through cold LN2 Trap 1 to fridge, both sides. Then isolate the sides and circulate with V6 open partially and mix open to dump. V9, V13b, V12b+speedi, V1, Condenser speedi, Still gate valves open, 3He pump on. Open V6 to 12.6%.
1330 P1(Condenser) → 0.32 mbar.
1330 Try closing V12a speedivalve. G1 falls as it should, showing we have throughput. Falls at 10.4 mbar/min . Open V12a speedivalve again.
1335 Let 5.4 mbar He exchange gas into IVC.
1345 MC(Cernox) = 296.4 K, Sorb = >249 K (max), IVC = 5.4 mbar, G2/G1/P1 (circulation) = 669/738/0.8 mbar, Level resistor = 0.980 kΩ.
1350 Begin LN2 transfer
1355 Tower thermometer / Goldman thermometer = 1.0013/2.0373 kOhm.
1400 MC(Cernox) = 295.8 K, Sorb = >249 K (max), IVC = 5.4 mbar, G2/G1/P1 (circulation) = 669/738/1.5 mbar, Level resistor = 1.051 kΩ.
1400 Close V12a speedivalve for 2 minutes to assess throughput. (Condenser pressure G1 should fall.) G1 falls at 14.6 mbar/min. Open V12a speedivalve again.
1430 MC(Cernox) = 247.1 K, Sorb = >249 K (max), IVC = 3.0 mbar, G2/G1/P1 (circulation) = 669/736/8.0 mbar, Level resistor = 1.227 kΩ. Tower/Goldman = 1.0023/2.0425 kΩ.
1430 Close V12a speedivalve for 2 minutes to assess throughput. (Condenser pressure G1 should fall.) G1 falls at 18.2 mbar/min. Open V12a speedivalve again.
1455 Transfer is going fast, no need to pressurize the LN2 Dewar this time (same as last time). Gauge on Dewar = 8.5 PSI
1500 MC(Cernox) = 172.4 K, Sorb = 236 K, IVC = 2.2 mbar, G2/G1/P1 (circulation) = 665/732/off_scale mbar, Level resistor = 1.333 kΩ. Tower/Goldman = 1.0067/2.0603 kΩ.
1500 Close V12a speedivalve for 2 minutes to assess throughput. (Condenser pressure G1 should fall.) G1 falls at 32.8 mbar/min. Open V12a speedivalve again.
1530 MC(Cernox) = 133.2 K, Sorb = 159 K, IVC = 1.9 mbar, G2/G1/P1 (circulation) = 657/722/off_scale mbar, Level resistor = 1.329 kΩ. Tower/Goldman = 1.0142/2.0868 kΩ.
1530 Close V12a speedivalve for 2 minutes to assess throughput. (Condenser pressure G1 should fall.) G1 falls at 47.6 mbar/min. Open V12a speedivalve again.
1545 Stop LN2 transfer. Close LN2 Dewar valve. Pull out Level Resistor and put stopper in port. Put ping-pong ball on MB exhaust port.
1545 Close V6 and turn off 3He pump.

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