2018/04/23 (Monday)
| Warming up after a short appeared at 77K. Also throughput was poor. Pumping out cryostat vacuum jacket. | |
| 0845 | Turbo = 4.6 nbar, cryostat vacuum jacket = 120 nbar with turbo valved out |
| 0845 | MC(Cernox) = 275.7 K |
| Notes on channel with the short: |
- Short was DIB3pA QET to chassis. This is Side2pB.
- Short was present at 77K, started to disappear at 100 K. Not present at room temperature.
- During tower assembly this channel also shorted to chassis but messing with the DIB connection fixed it.
- This channel showed significantly higher resistance on the bench than the last check after Run 62. All other channels were close to the old values.
- The wirebonds on this channel are quite long. In order to make this an operational channel it was bonded to two stadiums of the B-ring, jumping over the A-ring.
- In Run 62 tower assembly there were multiple times that channels shorted to chassis, though I'm not sure whether this particular one did.
- Since pushing the DIB in at room temperature caused a short, probably making the bond bow up and hit the crown, seems reasonable that something similar happens upon cooling, when the housing shrinks more than the crystal and pushes the DIB closer.
- Could try simply pushing the bonds down a bit, has worked in the past, as long as this doesn't break the bonds.
- The bonding for this channel was meant to make it a readable channel. Since we probably won't look at Side2 this run, could consider jump-bonding this to another Side2 channel, simpler and more reliable bond.
- UPDATE - it wasn't the detector, it was the side coax - see April 27
| 0930 | Check fridge pressures: LHe trap, Condenser ~ 0.3 mbar, Still ~ 0 mbar. Pump out with scroll pump. |
|---|---|
| Throughput test procedure, Cold Trap 2: |
- All mixture in dump, LN2 traps cold, condenser & still valves open (3He pump on - optional)
- Open V9, V13b, V12b+speedivalve, V3. Wait for G1 to be close to G2.
- Close V12b+speedivalve and V3, open V1
- monitor G1
| 0945 | Perform mixture throughput test at MC = 276 K using above procedure. Let G1 rise to 567 mbar before Step 3, then it falls to 41 mbar, then rises steadily. Throughput 7.1 mbar/min. A little worse than Run 63. |
|---|---|
| 0935 | Lower main bath |
| 1005 | IVC open, beginning disassembly. The SQUET on DIB4 has a very bent pin, Pin 42, SQUID D return. This is Side1pF, so it's necessary. This connection showed no problems in checkouts though. |
| 1020 | Fiddle with the SQUET on DIB3, which seems to have bad pins and sometimes shows bad connections in phonon-related lines. Can cause various channels to come and go, including pC, the one that we need. Maybe the solder connections of the pins are a little loose and can be improved? |
| 1130 | On the bench we found that on ZC-74, Pin 27 (SQUID B bias) was bad, moving it a little caused the resistance to jump to MΩ. Tried heating this pin to rewet the solder - after this it seemed more stable at first but a little stress caused it to go bad as before. Tried removing this pin completely and soldering in a new one - now it's completely open. Not good. |
| Tested SQUET ZC-23 on bench. Same result as in the cold hardware page, SQUID A reads open but everything else OK. This SQUET has all four shunt resistances reduced to 6.7 mΩ. We'll try it as a replacement for ZC-74. | |
| 1333 | Removed adaptor plate from tower |
| 1335 | Look at DIB3pA-to-chassis. No short. Try pushing in the side coax at the DIB - can make the short appear, kind of unstable. |
| 1340 | Remove side coaxes |
| 1350 | Remove detector. Inspect Side2 DIB3 (note this is the top, source-side). It's clear that the very long bond on Pin 2 is bowing up, clearly coming close to the source plate. Try pushing down on it to bend it flatter. Wound up breaking it off at the DIB. So, just pulled it off completely. The Pin 1 bond is still good - still shows continuity to DIB3pB. |
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| 1410 | Reassemble tower and replace side coaxes. |
| 1410 | Tower electrical check: |
| Detector | S101 | DIB | 1 | |
|---|---|---|---|---|
| side coax | ST-3-3 | date/who: | 2018-04-23 | GR MF |
| face | 5 | |||
| +lead | - lead | signal | typical | previous/now |
| 1 | 2 | QET A | 100 to 200 Ω | 401/399 Ω |
| 2 | 4 | QETA-B | 100 to 200 Ω | 2.7/3.1 kΩ |
| 3 | 4 | QET B | 100 to 200 Ω | 209/208 Ω |
| 4 | 6 | QETB-C | 100 to 200 Ω | 5.9/OL kΩ |
| 5 | 6 | QET C | 100 to 200 Ω | 494/492 Ω |
| 6 | 8 | QETC-D | 100 to 200 Ω | 3.9/4.2 kΩ |
| 7 | 8 | QET D | 100 to 200 Ω | 376/375 Ω |
| 2 | 8 | QETA-D | 100 to 200 Ω | 3.2/3.5 kΩ |
| 9 | chassis | LED1 Rforward | 8 to 9 MΩ | 94/150 kΩ |
| 9 | chassis | LED1 Vforward | 1.0 to 1.1 V | 1.04/1.04 V |
| chassis | 9 | LED1 Rreverse | <1 nS | 275/240 kΩ |
| 10 | chassis | LED2 Rforward | 8 to 9 MΩ | 756/800 kΩ |
| 10 | chassis | LED2 Vforward | 1.0 to 1.1 V | 1.117/1.114 V |
| chassis | 10 | LED2 Rreverse | <1 nS | 0.2/0.2 nS |
| All pins → Ground | <1.0nS | (Except for LED pins) | all <0.3/0.5 nS | |
| Detector | S101 | DIB | 3 | |
|---|---|---|---|---|
| side coax | ST-3-9 | date/who: | 2018-04-23 | NM MF |
| face | 3 | |||
| +lead | - lead | signal | typical | previous/now |
| 1 | 2 | QET A | 100 to 200 Ω | 280/OL Ω |
| 1 | 4 | QETA-B | 100 to 200 Ω | 2.7 kΩ |
| 3 | 4 | QET B | 100 to 200 Ω | 129/129 Ω |
| 4 | 6 | QETB-C | 100 to 200 Ω | 3.19/3.3 kΩ |
| 5 | 6 | QET C | 100 to 200 Ω | 132/132 Ω |
| 6 | 8 | QETC-D | 100 to 200 Ω | inf/inf Ω |
| 7 | 8 | QET D | 100 to 200 Ω | inf/inf Ω |
| 2 | 8 | QETA-D | 100 to 200 Ω | inf/inf Ω |
| 9 | chassis | LED1 Rforward | 8 to 9 MΩ | 790/790 kΩ |
| 9 | chassis | LED1 Vforward | 1.0 to 1.1 V | 1.098/1.087 V |
| chassis | 9 | LED1 Rreverse | <1 nS | 0.3/0.1 nS |
| 10 | chassis | LED2 Rforward | 8 to 9 MΩ | 790/790 kΩ |
| 10 | chassis | LED2 Vforward | 1.0 to 1.1 V | 1.099/1.089 V |
| chassis | 10 | LED2 Rreverse | <1 nS | 0.2/0.3 nS |
| All pins → Ground | <1.0nS | (Except for LED pins) | all <0.3/0.3 nS | |
| Detector | S101 | DIB | 4 | |
|---|---|---|---|---|
| side coax | ST-3-10 | date/who: | 2018-04-23 | NM MF |
| face | 1 | |||
| +lead | - lead | signal | typical | measured |
| 1 | 2 | QET A | 100 to 200 Ω | 458/457 Ω |
| 2 | 4 | QETA-B | 100 to 200 Ω | 4.33/4.5 kΩ |
| 3 | 4 | QET B | 100 to 200 Ω | 526/525 Ω |
| 4 | 6 | QETB-C | 100 to 200 Ω | open (flashing OL) |
| 5 | 6 | QET C | 100 to 200 Ω | 453/452 Ω |
| 6 | 8 | QETC-D | 100 to 200 Ω | 5.4/6.1 kΩ |
| 7 | 8 | QET D | 100 to 200 Ω | 483/482 Ω |
| 2 | 8 | QETA-D | 100 to 200 Ω | 6.22/flashing OL kΩ |
| 9 | chassis | LED1 Rforward | 8 to 9 MΩ | open/open kΩ |
| 9 | chassis | LED1 Vforward | 1.0 to 1.1 V | 1.093/open V |
| chassis | 9 | LED1 Rreverse | <1 nS | 0.1/0.4 nS |
| 10 | chassis | LED2 Rforward | 8 to 9 MΩ | 787/800 kΩ |
| 10 | chassis | LED2 Vforward | 1.0 to 1.1 V | 1.095/1.084 V |
| chassis | 10 | LED2 Rreverse | <1 nS | 0.1/0.4 nS |
| All pins → Ground | <1.0nS | (Except for LED pins) | all <0.2 nS | |
| 1600 | Tower reassembly complete |
|---|---|
| 1635 | Installing tower, 100mK stage started |
| 1720 | DIB3 SQUET plugged in. Electrical checkout OK. (SQUID A open, we knew that already.) |
| 1730 | DIB1 SQUET plugged in. Electrical checkout OK. |
| 1740 | DIB4 SQUET plugged in. Electrical checkout OK. |
| 1740 | Cross-channel checks on all 3 DIBs, all channels show continuity to at least one other channel. |
| 1800 | Start pumping IVC with scroll pump |
| 1810 | Start pumping IVC with turbo pump |
| Cryocleaning mixture | |
|---|---|
| 1005 | Start cryocleaning mixture through cold LN2 Trap 2, V6 = 13.0% |
| 1010 | Increase V6 to 13.1% to speed up flow |
| 1020 | Increase V6 to 13.2% to speed up flow |
| 1040 | Increase V6 to 13.3% to speed up flow |
| 1110 | Stop cryocleaning, Trap 2 65 minutes. Pump mixture to dump. |
| 1120 | Start cryocleaning mixture through cold LN2 Trap 1, V6 = 12.9% |
| 1125 | Increase V6 to 13.2% to speed up flow |
| 1145 | Increase V6 to 13.3% to speed up flow |
| 1245 | Stop cryocleaning, Trap 1 85 minutes. Pump mixture to dump. |
| 1315 | Check pressure in warm LN2 Trap 2: 19.4 mbar. Pump out with scroll pump |
| 1325 | Start cryocleaning mixture through cold LN2 Trap 2, V6 = 12.9% |
| 1425 | Increase V6 to 13.2% to speed up flow |
| 1535 | Stop cryocleaning, Trap 2 130 minutes. Pump mixture to dump. |
| 1730 | Check pressure in warm LN2 Trap 1: 3.4 mbar. Pump out with scroll pump |
| 1745 | Check pressure in warm LN2 Trap 2: 9.0 mbar. Pump out with scroll pump |

