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2018/04/17 (Tuesday)

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Status: LN2 transfer yesterday. Mixture cleaned several times.
0900 MC(Cernox) = 77.3 K, Sorb = 126 K, IVC = 1.6 mbar, G1 (fridge) = 598 mbar.
0900 Start pumping out IVC with scroll pump, then turbo pump
0935 Try Mini-throughput check: close off Trap 2 and V3. Only V1, condenser speedivalve, still gate valve, and V9 open. Turn on 3He pump, then open V6 to 12.8%. This pumps mix out of the still side and we can see if the pressure goes down on the condenser side. G1 (condenser) started out at 598 mbar, but did not fall. Looked like a blockage… BUT then discovered that the gate valve to the still was not open. So ok, not a good test. Let's do a standard throughput test.
Throughput test procedure, Cold Trap 2:
  1. All mixture in dump, LN2 traps cold, condenser & still valves open (3He pump on - optional)
  2. Open V9, V13b, V12b+speedivalve, V3. Wait for G1 to be close to G2.
  3. Close V12b+speedivalve and V3, open V1
  4. monitor G1
1000 Perform mixture throughput test at MC = 77 K using above procedure. Let G1 rise to 585 mbar before Step 3, then it falls to 75 mbar, then begins to rise. Throughput 48.0 mbar/min. Close to Run 67.
Cryocleaning log
date trap duration (minutes) contaminants removed (mbar)
Apr 6 1 70 9.5
Apr 6 2 70 6.6
Apr 6 1 70 11.0
Apr 6-7 2 overnight, no circ, dump exposed to trap 12.8
Apr 7-9 1 overnight, no circ, pump exposed to trap 6.8
Apr 9 2 70 8.9
Apr 9 1 60 9.0
Apr 10 2 90 10.5
Apr 10 1 70 8.5
Apr 10 2 75 6.6
Apr 10 1 70 1.9
Apr 11 2 75 2.7
Apr 11 1 75 14.4
Apr 11 2 70 4.5
Apr 11 1 70 6.4
Apr 12 2 70 4.7
Apr 12 1 135 3.3
Apr 16 2 95 4.0
Apr 16 1 60 14.7
1140 Electrical check at 77K on DIB3: good except Feedback C is 31 kΩ and unstable, should be 7-9 kΩ. Bad because this is a connected Side1 channel, Side1pA. Check cross-channel resistances: >10 GΩ except A-C is 30 MΩ. That's Side2 to Side1. But A-B is Side2-Side2, so it should be lower than A-C, and B-C should be about the same as A-C. So maybe QETB is not connected at the detector. That's Side2pA, so that would be bad for biasing purposes.
1155 Electrical check at 77K on DIB4: good except short from qI FET gate to chassis, not relevant to this run. Cross-channel checks show continuity - pattern is a little odd but there's continuity. Lowest cross-channel is A-B (side2-side2) at 2 MΩ.
1205 Electrical check at 77K on DIB1: all good. Cross-channel checks show, at least from B to each of the others.
so the biggest concerns are:
DIB3pC (Side1pA) Feedback has somewhat higher resistance than it should, could be bad pin at SQUET
DIB3pB (Side2pA) may not be connected at the detector, problem for biasing (but hard to say whether it's connected or not)
1210 Double-checked DIB3, now the iffy Feedback C reads fine. Should check phonon-related DIB3 connections again, see if they stay stable. Also cross-channel checks look OK now, at least A-C and B-C have continuity.
1225 Stop pumping IVC with turbo and start leak detector on IVC. Background leak = 500 pbarL/s.
1230 Leak detector on IVC = 640 pbarL/s
1235 Begin blowing out LN2. Main bath (G3) = 460 mbar above 1atm.
1235 Leak detector on IVC = 640 pbarL/s
1240 LD = 640 pbarL/s. Main bath = 466 mbar.
1250 LD = 620 pbarL/s. Main bath = 454 mbar.
1251 Main bath pressure starts falling
1300 LD = 2300 pbarL/s. Main bath = 155 mbar.
LD climbing… hits 20,000 pbarL/s
1305 LD = 6000 pbarL/s. Main bath = 140 mbar. Not sure why leak is coming back down.
1310 LD = 1200 pbarL/s. Main bath = 125 mbar. Stop pressurizing main bath.
1310 Leak signal rises again after stopping the He pressure. Don't know why. Climbs up to around 100,000 pbarL/s
1320 LD = 130,000 pbarL/s.
1325 Start pumping main bath with scroll pump. LD goes down.
1330 LD = 5,000 pbarL/s. Main bath pumping out slow, still around 0.4 bar. I think there's still LN in there (He cylinder was low).
1330 LD = 1400 pbarL/s.
Stop pumping out main bath. Restart LN2 blowout.
1335 Oops - I think the blowout was finished after all. The problem was that I didn't disconnect the hose from the LN2 transfer tube and insert a stopper. Dumb.
1340 Start pumping main bath with scroll pump. Leak falls.
1350 LD = 980 pbarL/s. Main bath = 0.45 mbar.
1350 Pump on IVC with turbo pump for a bit, try to get the leak background lower. Then close it again.
1355 LD = 670 pbarL/s. Main bath = 0.22 mbar.
1355 Try squirting He around stripline tube elbow. Causes increase in leak signal, around 700→800 pbarL/s.
1400 Pump out 1K Pot with scroll pump
1400 Close scroll pump valve.
Let 1 hose-length of He into IVC through vent. Main bath 0.5→1.6 mbar. Leak increases, 650→850 pbarL/s
1405 Let 1 more hose-length of He into IVC through vent. Main bath →3.0 mbar. Leak increases, 870→1100 pbarL/s
1420 Fill main bath with N2 gas. (Also pump IVC with turbo pump to bring leak baseline down.) LD base winds up at 720 pbarL/s after closing off turbo again.
1430 Squirt a blast of He gas down the LN2 transfer tube. Leak 720→1400 pbarL/s
1435 Raise transfer tube ~1 cm, then do another He squirt. Leak 1610→1630 pbarL/s
1435 Push transfer tube down again then squirt a blast of He gas down. Leak 1610→2700 pbarL/s
As on March 15 it looks like there must be a leak in one of the lower IVC seals. Maybe not as bad as then, but in this run it's less tolerable because superfluid He films on the detector would cause phonon noise.
Looks like we need to warm up.
1450 Let 8.6 mbar He transfer gas into IVC.
1500 Disconnect vacuum manifold from IVC port then connect to cryostat vacuum jacket port, then pump out line with scroll pump.
1505 Let 100 mbar N2 gas into vacuum manifold. Then open cryostat vacuum jacket valve to let this into the vacuum jacket.
1510 MC(Cernox) = 82.2 K, Sorb = 146.3 K, Cryostat outer surface = 22.9 C
1505 Let another 100 mbar N2 gas into cryostat vacuum jacket. (Fill hose with N2, then open green valve on pump manifold, leaving cryostat vacuum jacket valve open. 13 tube-lengths = 100 mbar @ manifold.) Cryostat vacuum jacket pressure = 8.6 mbar.
1515 MC(Cernox) = 83.5 K, Sorb = 149.0 K, Cryostat outer surface = 22.5 C
1515 Pump mixture out of fridge and cold LN2 Trap 2 to dump.
1520 MC(Cernox) = 84.6 K, Sorb = 151.6 K, Cryostat outer surface = 22.0 C
1530 MC(Cernox) = 86.4 K, Sorb = 157.4 K, Cryostat outer surface = 21.4 C
1615 MC(Cernox) = 95.1 K, Sorb = 185.4 K, Cryostat outer surface = 20.0 C
1640 MC(Cernox) = 100.6 K, Sorb = 199.6 K, Cryostat outer surface = 19.8 C
Warming time constant is around 15 hours. Should reach 273 K around midnight tomorrow night.
1700 MC(Cernox) = 105.1 K, Sorb = 210.8 K, Cryostat outer surface = 19.7 C
1845 MC(Cernox) = 126.8 K
2145 MC(Cernox) = 157.7 K

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