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2018/05/16 (Wednesday)

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Status: Initial LHe transfer yesterday
0905 MC(Cernox)/Sorb/1K Pot = 4.9/8.7/6.7 K, G1(fridge) = 545 mbar, MB = 51.6%
0905 Turbo on IVC = 1.4 nbar
0910 Fill LN2 cold trap bath
0915 Check pressure in 1K Pot: 2.5/30 bar on mechanical gauge. Pump out with scroll pump. Falls from 6.7→6.53 K, 0.4 mbar
0925 Switch to pumping 1K Pot with 4He pump. When we closed off the pump to do the switch, the pot pressure rose back up off-scale on p2 to something like 2.5/30 bar again.
open 4He pump exhaust to recovery and open red recovery valve
0925 1K Pot = 6.55 K / 0.28 mbar
0927 Open needle valve several degrees. No change in pot pressure; temperature actually goes up at first to 6.7 K, then after half a minute starts to fall very quickly, must have got some LHe in there
0930 1K Pot = 4.74 K / 0.30 mbar, temperature still falling
0935 1K Pot = 4.78 K / 0.32 mbar
0950 Have tried opening the needle valve. Pressure does not increase. Temperature continues to rise. Open the needle valve completely, many rotations. The temperature is well above 4K, has risen back to 6.5 K = why?? Like no LHe is going in. But earlier we got it to fall to 4.7 K, as if some LHe was going in.
1100 Leaving the 1K Pot alone for a while, it went through some oscillations. The 4He pump is pumping on it and the needle valve is closed. Temperature fell from 6.6 K to 5.3 K then rose to 6.2 then fell to 5.8 etc, like a damped oscillator.
1105 With needle valve completely closed, close off pump and see how fast pressure rises:
minutes mbar (P2)
0 0.3
0.5 6
1.0 27
1.5 120
1.8 1000 (off-scale)
1130 Discussing with Paul Crowell, he says the symptoms strongly suggest that it's plugged. One piece of evidence is that when we close off the pump and open the needle valve wide, the pressure only goes up a few inHg, instead of rising to 1 atm. Another symptom is that pressure doesn't really increase when you are pumping even if you have the needle valve wide open.
Paul suggests removing the needle valve shaft completely. If it is opened enough turns the shaft becomes loose and can be pulled straight up. There are o-rings at the top on the shaft that seal the shaft from atmosphere - these may be worn out and need replacement. He also said that there is an extender on the fill tube that can be unscrewed, if we want to look at that. Of course we need to warm up to do that.
1155 Try another test to see how fast the 1K Pot pressure rises when the pump is closed off, but this time with needle valve open 5 full rotations:
minutes mbar (P2)
0 0.28
0.5 6.5
1.0 36
1.5 1000 (off-scale)
so it goes up a little faster with needle valve wide open. Only goes up to 2/30 bar on mechanical gauge.
1205 Close 1K Pot needle valve and speedivalve. Close off valve to 4He pump and turn off pump. Close recovery valve.
1205 Stop pumping IVC with turbo. IVC pressure = 14 nbar
1215 Let 2 hose-lengths He into IVC. IVC → 100 ubar. MC and 1K Pot temperatures fall to ~4.5 K
1230 MB = 47.0%. Recovery rate = 178 sec/sqft
1235 Let 1.9 mbar He gas into vacuum manifold. Then open cryostat vacuum jacket valve to let this into the vacuum jacket. Vacuum jacket → 46 μbar
Recovery rate → 30 sec/sqft
1240 MB = 45.4%. Recovery rate = 15.5 sec/sqft
1250 MB = 42.1%. Recovery rate = 16.0 sec/sqft
1330 MB = 33.8%. Recovery rate = 31 sec/sqft
1330 Cryostat vacuum jacket = 7.4 μbar (it's drifted down)
1335 Let 1.9 mbar He gas into vacuum manifold. Then open cryostat vacuum jacket valve to let this into the vacuum jacket. Vacuum jacket → 34 μbar
1340 MB = 32.3%. Recovery rate = 21 sec/sqft
1410 MB = 22.9%. Recovery rate = 18 sec/sqft
1435 MB = 16.4%. Recovery rate = 21 sec/sqft
1455 MB = 11.7%. Recovery rate = 21 sec/sqft
1520 MB = 6.4%. Recovery rate = 20.5 sec/sqft
1540 Pump mixture to dump
1600 MB = -1.0%. Recovery rate = 28 sec/sqft
1600 Cryostat vacuum jacket = 14 μbar
1600 Let 2.2 mbar He gas into vacuum manifold. Then open cryostat vacuum jacket valve to let this into the vacuum jacket. Vacuum jacket → 40 μbar
1605 MC(Cernox)/1K Pot/Sorb = 4.4/5.2/6.6 K. Pot and Sorb rising steadily.
1750 MC(Cernox) = 13 K
1920 MC(Cernox) = 42.2 K
1950 MC(Cernox) = 47.44 K

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