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2016/07/21 (Thursday)

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Setup: iZIP mode, DIB1/2/3 → cables → 3.2 MHz filters → DCRC55(1)/33(2)/50(3)
DCRCs on overnight taking Ba data. Note: fridge was cooled below Al transition with mu-metal shield lowered 32.3 cm.
Fridge failure: 1K Pot ran dry at 4:06 am, from 1.4K/1.4mbar → 1.7K/1.0mbar. It was already down to 1.5 mbar by 9am. By 7:00 Tower had risen to 0.4 K, G1/G2 circulation pressures were around 900 mbar, P1 circulation pressure at 0.5 mbar. 1K Pot up to 4.7 K.
0725 close V6. G1/G2 fall to 500 mbar, 1K Pot temperature falls to 3 K, Tower rises to 3.6 K.
0730 Close V13a with G2 at 658 mbar - this much mixture now isolated in pump. Turn off 3He pump.
0735 G1 falls to 400 mbar then starts to rise again. Open 1K Pot needle valve a few degrees.
0740 Lower mu-metal shield to 37.8 cm below standard position
0740 1K Pot = 2.32 K / 8 mbar, falling slowly. G1 = 480 mbar, was rising, now flat. Tower = 3.9 K and flat.
0745 Fill LN2 cold trap bath
0750 1K Pot is hanging around 2.35 K. Can we try starting circulation?
0750 Turn on 3He pump. Open V13a. G1/G2 → 575/530 mbar. 1K Pot rises a little, → 2.64 K / 6 mbar. Pressure lowish: open needle valve a little more.
0800 Open V6 to 13.4%. G1/G2 were at 480/520 mbar, now rising. Peak at 560/510 mbar, now falling.
Still = 4.5 K
0802 Open V6 to 13.6%. G1/G2 rise too quickly. Close V6 before G1 reaches 950 mbar. Pressures falling.
0805 Open V3 to get pressures low (letting mixture expand into still pumping line). Pressures stabilize at G1/G2 = 535/495 mbar. Close V3 again.
0810 Open V6 to 13.4% again. But pressures go too high. Close V6 again and open V3.
0815 Crank 1K pot needle valve open more, finally it falls below 2 K. 1K Pot = 1.91 K / 45 mbar. G1/G2 start to fall. Let it settle.
0817 Main Bath (MB) = 72.1%. Good boiloff rate, nice and slow. Pattern of releasing pressure yesterday (5min, then 30min, then 60min after fill) worked.
0820 G1/G2 = 395/360 mbar, still falling. 1K Pot = 1.86 K / 20 mbar.
0830 G1/G2 = 380/345 mbar. Try circulating again. Tweak 1K Pot needle valve open more. Open V6 to 13.2%, G1/G2 go up to 440/410 mbar then fall again.
0840 G1/G2 = 320/295 mbar, falling. Open V6 to 13.4%. 1K Pot rise above 2 K so tweak it open again, drops back to 1.8 K. G1/G2 peak at 510/470 mbar then fall again.
Still = 3.8 K
0855 G1/G2 = 375/350 mbar, falling. Open V6 to 13.6%. 1K Pot has slowly risen above 2 K so tweak it open again, drops back to 1.8 K. G2 looked looked like it would stop at 710 mbar but then rose again because pot high again, annoying. Tweak pot again. G1/G2 peak at 750/700 mbar then fall again flatten.
0905 1K Pot climbs above 2K, tweak needle valve again. Each time this happens, opening the needle valve more causes the pot temperature to fall. Pressure goes up but then falls off, and another temperature increase happens. The pressure at which this occurs keeps getting higher: 10, 15, 15, 30, 40 mbar. Troubling.
0910 Still = 3.6 K. G1/G2 = 735/685 mbar, falling slowly. Too high to try opening V6 more. Open V4 for a minute to release condenser pressure into dump.
0915 G1/G2 = 515/480 mbar, climbing slowly. Open V6 to 13.7%. G1/G2 rise slowly, to 705/655 mbar in 5 minutes. 1K Pot needs tweaking again, at pressure of 30 mbar.
0925 G1/G2 flat at 720/670 mbar. Open V4 again to release some pressure. G1 falls to 420 mbar while V4 open, that is presumably the dump pressure. Close V4, pressures rise somewhat.
0930 G1/G2 = 595/560 mbar. Open V6 to 13.8%. 1K pot needs another tweak at 30 mbar. G1/G2 rise to 760/710 mbar.
0935 Open V4 again to release pressure, G1 fall to 460 mbar, close V4.
0940 G1/G2 = 645/605 mbar. Open V6 to 13.9%. Was hoping that the still pressure would come down, no luck. Everything is too warm.
0945 Another 1K Pot tweak, at 30 mbar again
0950 OK this isn't working. Need to investigate the pot. Stop circulation: close V6 & V13a, open V3. 1K Pot surge then settles at 1.74 K / 26 mbar.
0955 Tower/MC/Still = 3.4/3.3/4.8 K. At least Tower has gone down. Should let 1K Pot try to cool these. (Why is Still so high??)
1015 Tower/MC/Still = 3.4/3.4/4.1 K. OK, maybe Still is cooling slowly.
1020 Noticed IVC = 220 nbar. Was 12 nbar on the 13th after pumping out after the first LHe transfer. Try pumping with turbo.
1025 Open V13a to let mix from pump into fridge. Surge in 1K Pot temperature. Pot had been pretty stable for a while, down to about 1.7 K, pressure had decreased to 15 mbar.
1030 1K Pot = 1.75 K / 9.5 mbar, tweak needle valve again. After this Still temperature starts falling, and fridge pressure too, that's encouraging.
1045 Tower/MC/Still = 2.4/2.7/2.3 K. 1K Pot and Still and Fridge pressures were all decreasing together, then flattened. 1K Pot = 1.58 K / 7 mbar, kinda low, should it be tweaked again?
1050 Open V9 to let dump mixture into fridge. 1K Pot temperature and pressure surge.
1100 Tower/MC/Still = 2.25/2.47/2.21 K, G1/G2 = 85/100 mbar, 1K Pot = 1.62 K / 12 mbar. Pot and G1/G2 have been decreasing for the last 10 minutes.
1105 Close V9, leaving 76 mbar in dump. Close V3. Begin opening V6. At 13.0%, G2 starts to increase. 1KPot down to 1.54 K / 5 mbar, tweak open more.
1110 IVC pumping pressure down to 1.2 nbar. Close valve to pump. IVC = 7.4 nbar.
1115 G1/G2 = 80/75 mbar and falling. 1K Pot = 1.71 K / 40 mbar. Open V6 to 13.2%.
1120 Tower/MC/Still = 2.16/2.41/2.19 K
1130 G1/G2 = 110/105 mbar and flattish. 1K Pot = 1.68 K / 24 mbar. Open V6 to 13.4%.
1140 G1/G2 = 205/190 mbar and flattish. 1K Pot = 1.66 K / 19 mbar. Open V6 to 13.6%.
1150 G1/G2 = 300/280 mbar and flattish. 1K Pot = 1.64 K / 15 mbar. Open V6 to 13.8%.
1155 G1/G2 = 365/342 mbar and flattish. 1K Pot = 1.63 K / 13 mbar. Open V6 to 14.0%. P1 begins dropping.
1200 Tower/MC/Still = 1.26/1.43/1.67 K
1205 G1/G2 = 370/345 mbar and falling, P1 = 7 mbar. 1K Pot = 1.62 K / 12 mbar. Open V6 to 14.2%.
1210 G1/G2 = 305/285 mbar and falling, P1 = 2.8 mbar. 1K Pot = 1.61 K / 11 mbar. Open V6 to 100%.
1215 Tower/MC/Coldplate = 1.11/1.03/0.83 K, Still = 1.31 K / 0.22 mbar, G1/G2 = 325/305 mbar, 1K Pot = 1.61 K / 9.5 mbar
1230 Tower/MC/Coldplate = 87/70/174 mK, Still = 1.38 K / 0.15 mbar, G1/G2 = 275/255 mbar, 1K Pot = 1.61 K / 9.5 mbar
1300 Tower/MC/Coldplate = 40.4/30.4/157 mK, Still = 1.39 K / 0.11 mbar, G1/G2 = 200/190 mbar, 1K Pot = 1.57 K / 6.5 mbar
at some point, mu-metal shield was raised to its standard position
1315 Tower is at 37.4mK. All pulses look good after messing with Driver Offsets. Start a 30min background series at -4/+4 V with FG=5/2/5, OG=8/3/8, with 1000 initial randoms, 1000 ending randoms, with 30s flash and 25 minute cooldown between series. Trigger on DIB1 phA with threshold of 30ADC bins, with 150 us pileup cut window.
1415 Series finished. Close V6 to commence warm up procedure.
1420 V6 is closed. Close V13A and turn off He3 pump. Turn MC Heater to 1mW.
1445 We've skipped the step of opening V3, doesn't really seem necessary.
Tower = 1.1 K & rising, G1 = 25 mbar and falling slowly, P1 = “1000”
1454 Tower/MC/Coldplate = 1.38/1.52/1.00 K
1510 Tower/MC/Coldplate = 1.61/1.78/1.51 K. It may be behaving differently with V3 closed. Last two times, Tower jumped up at around 40 minutes after beginning heating. We are at the 50 minute mark.
1525 Tower/MC/Coldplate = 1.79/1.96/2.07 K
1530 1K Pot = 1.50 K / 4.5 mbar, tweak open before cooling
1535 Turn on He3 pump, and open V13A. G1/G2 rise to 89/87 mbar, then settle downward.
1540 Open V6 to 13.2% and G1/G2 begin rising.
1555 G1/G2 = 80/76 mbar and flattish. 1K Pot = 1.61 K / 9.5 mbar. Open V6 to 13.4%.
1610 G1/G2 = 113/107 mbar and flattish. 1K Pot = 1.59 K / 8.0 mbar. Open V6 to 13.7%.
1625 G1/G2 = 299/281 mbar and flattish. 1K Pot = 1.56 K / 6.0 mbar. Open V6 to 13.9% and P1 starts dropping.
1630 Filled HPGe dewar
1635 G1/G2 = 383/359 mbar and flattish. 1K Pot = 1.56 K / 6.0 mbar. Open V6 to 14.1% and P1 keeps dropping.
1640 G1/G2 = 445/416 mbar and flattish. 1K Pot = 1.57 K / 6.5 mbar. Open V6 to 14.3%.
1642 Not much change. Open V6 to 14.5%, then 14.9%, then all the way.
1657 1K Pot = 1.48 K / 4.0 mbar. Tweak open. Tower temperature at 991mK and dropping.
1720 G1/G2 = 348/326 mbar. 1K Pot = 1.69 K / 32 mbar. The MC Heater was still on, which was keeping the Tower at ~700mK. Turning it off dramatically increases cooling rate.
1721 Fill LN2 cold trap full.
1755 Tower temperature at 37.4 mK. 1K Pot at 18mbar, so tweak it open so we're good for overnight.
Cooled below 1.2 K Al transition with mu-metal shield in standard position
1800 Check phonon channels. Adjusting the Driver Offsets brings all channels alive.
1810 Start 12 hours of 30min background series at -4/+4 V with FG=5/2/5, OG=8/3/8, with 1000 initial randoms, 1000 ending randoms, with 30s flash and 25 minute cooldown between series. Trigger on DIB1 phA with threshold of 30ADC bins, with 150 us pileup cut window.

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