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2016/05/28 (Saturday)

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Status: LN in MB. IVC turbo pumping overnight.
1000 IVC = 3.4 e-6mbar pumping, 40 e-6mbar with pump valved out
1005 LD = 0.44 e-9mbarL/s. Open LD to IVC, LD = 360 e-9mbarL/s and falling
1030 Begin blowing out LN. G3 → 225 mbar. LD = 240 e-9 mbarL/s
1035 G3 drops to 150 mbar. Maybe LN already mostly gone.
1050 Stop LN blowout. Only gas coming out of tube into the bomb Dewar. LD = 240 e-9mbarL/s
1055 Start pumping out MB with scroll pump. LD rises to 560 e-9mbarL/s. This rise is normal.
1100 P2 (MB) = 0.28 mbar. LD falling now, 540 e-9mbarL/s
1110 Fill MB with He gas
1130 Put 4.6e-2 mbar He exchange gas into IVC. MC and Sorb temperatures increase.
1140 Check 1K Pot pressure: 26 mbar on P2. Evacuate 1K Pot
1200 Begin LHe transfer.
1200 MC = 94 K, Sorb = 206 K
1210 Begin pressurizing Dewar for transfer. Note 250L Dewar began with only 173 L, but probably this is sufficient.
1215 Sorb temperature starts to decrease, peaked at 208 K
1225 MC = 98 K and flat, Sorb = 203 K
1240 Tried turning on 3He pump - light goes on on GHS but pump does not turn on. Is circuit box switched off??
1245 MC = 92 K, Sorb = 160 K, IVC = 1.4e-2 mbar
1250 Reset pump power switchbox. On the box all the lights were off. I pressed the red button, Mains On, then the DC Fail light came on. Then I hit the white Reset button and the DC Fail light went off. Then I turned on the pump and it worked.
1300 With MC at 82 K perform throughput test. Unfortunately it looks like we have a blockage. G1 falls to 6.5 mbar and remains flat (zero throughput).
1320 MC = 71 K, Sorb = 79 K, IVC = 8.6e-3 mbar
1330 After pumping all mix to dump, perform another throughput test. MC = 67 K. G1 falls to 14 mbar barely rises over period of 5 minutes. Throughput ~ 0.3 mbar/minute. Blockage.
we really should a) pump fridge out before LN transfer and b) clean mixture before throughput test
1340 Stop LHe transfer. (Never should have started it.) Level still too low to register. Leaving MB-side of transfer stick in MB - maybe Taconis will boil off the LHe faster.
1345 MC = 60 K, Sorb = 20 K, IVC = 1.0e-2 mbar
1410 MC = 51 K, Sorb = 19 K (but now rising, hit a minimum of 16 K
1415 Fridge contents pumped to dump, down to P1 = 0.7 mbar, G1 = 2 mbar. Turn off 3He pump.
note I also pumped out LN2 Trap 1 and then put it in the LN2 Cold Trap Bath and filled the bath.

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