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2016/05/30 (Monday)

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Status: Fridge warming after blockage found
0940 MC = 170 K, Sorb = 250 K (flatline - looks like maximum), IVC = 1.4e-1 mbar
1045 Pump P1 volume to dump, down to P1=0.24 mbar. Then open Still gate valve. P1 jumps to 3.8 mbar. A lot of frozen air it seems.
1055 Fill LN2 storage Dewar
1100 Pump P1 volume to dump again, then open Condenser to P1. Goes up from 0.65 to 0.70 mbar. Open Still to P1 - pressure goes up a little more, to 0.90 mbar. Hard to say whether there's still a blockage.
1105 Fill LN2 cold trap bath. Trap 1 is in bath, Trap 2 is at room temperature.
1120 Pump still and condenser to dump, down to P1 = 0.38 mbar.
1145 Begin cryocleaning mixture through Trap 1. V6 = 12.8%
1150 G2 is rather high, 983 mbar. G1 is 638 mbar. Possibly the trap is full of contaminants and creating an impedance.
1155 Stop cryocleaning, pump mixture to dump.
1210 Stop pumping mixture to dump with Trap 1 (P1) down to 0.070 mbar. Dump (G2) = 790.3 mbar (current mixture amount). Remove Trap 1 from bath to let it warm up, monitor pressure on P1.
1240 Trap 1 nearly at room temperature. 9 mbar of contaminants in trap 1 (on P1). Start pumping trap contaminants out through vent with scroll pump.
1315 Trap 1 pumped down to 0.65 mbar on P1. That took a while, maybe it was still warming a bit. Trap at room temperature now. Close GHS valves and turn off scroll pump.
1325 Return Trap 1 to LN2 cold trap bath. Open V9 and V13a to expose mixture to cold trap overnight.

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