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2025/08/02 (Saturday)

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  • Lab in-personnel: Himangshu, Yan

^ Status | MC(Cernox) = 77.85 K; still = 71.7 K. IVC pumped out overnight.

0900 connect LD to the vacuum manifold. baseline level: 6e-8.
0930 Refill cold trap with LN container
0940 Throughput test

All mixture in dump, LN2 trap 1 is cold, condenser & still valves open (3He pump on - optional) Open V9, V8, V3, V5. Wait for G1 to be close to G2 (within 100 mbar). Close V3 and V5, open V1 monitor G1

0950 Perform mixture throughput test at MC = 77 K using above procedure with 3He pump on. Let G1 rise to ~500 mbar before Step 3, then it falls to ~50 mbar, then rises. Throughput = ~50 mbar/min (previously 25 mbar/min, but 2023 March measurement was 41 mbar/min, and 2021 measurement was 61 mbar/min).
1000 collecting mix back into dump.
1000 Preparing for LN blowout: https://zzz.physics.umn.edu/!cdms/cdms/k100/procedure/blow_out_ln2
1000 Switch from turbo to LD. baseline level: 8e-8
1040 Start blowing out LN. MB = 3 psi + atm.
1040 MC(Cernox) = 77.91 K. still = 71.3 K
1110 blowout finished. Only took 30 mins.. why?? LD rate 8e-8. MC(Cernox) = 77.94 K, still = 71.6 K
1120 Pumping out the MB using scroll.
1140 P2 is reading 0.1 mBar. Valve out scroll, p2 jumps to 0.8 mbar. Probably okay? Keep pumping.
1140 LD has been stable. Now at 5.5e-8. MC(Cernox) = 77.96 K, still = 71.8 K
1140 install Helium recovery bronze pipe (it had a leak and Mike (should have?) fixed it).
1200 Overpressurize MB to 2psi + atm.
1240 Add exchange gas to IVC. MXP (not to be trusted!) reads 180 mTorr = 239 uBar.
1255 Start LHe transfer.
1255 MC(Cernox) = 78.46 K; still = 72.5 K
1305 Put mix into the loop, but not circulating.
1310 MC(Cernox) = 65.43 K; still = 53.8 K, level meter =4%, MXP = 74 mTorr = 98 uBar, CC (Cold Cathode) = 5 mTorr = 6 uBar
1320 We trust the CC gauge more, which means we are short by a factor of 2 or 3. Added more exchange gas.
1325 MC(Cernox) = 52.63 K; still = 32.8 K, level meter =7%, MXP = 199 mTorr = 264 uBar, CC (Cold Cathode) = OL
1330 MC(Cernox) = 47.21 K; still = 24.0 K, level meter =20%, MXP = 168 mTorr = 223 uBar, CC (Cold Cathode) = OL
1330 Brought a helium cylinder as the one we've been using is running out.
1335 MC(Cernox) = 39.26 K; still = 20.3 K, level meter =32%, MXP = 153 mTorr = 204 uBar, CC (Cold Cathode) = OL
1345 MC(Cernox) = 28.81 K; still = 14.6 K, level meter =75%, MXP = 128 mTorr = 170 uBar, CC (Cold Cathode) = 10 mTorr = 13 uBar
1355 MC(Cernox) = 9 K, dropped directly from 17 K. Turn on turbo. level meter = 71%, the LHe tank is empty. stop He transfer.
1410 MC(Cernox) = 4.45 K, still = 6.0 K, level meter = 70%.
1440 Start pumping on 1K pot. 1K pot temperature dropped from 6 K to 3.1 K.
1500 Slowly opening up the needle valve. P2 is reading 5 mBar, 10 mBar, 15 mBar, 19 mBar, 30 mBar, 40 mBar. 1K pot final temperature 1.8 K.
1520 Start circulating mix with dump closed. slowly open V2 in steps: 1K pot pressure spike; G1 and G2 goes up too (kept under 650 mBar).
1540 Slowly open VT as well. did not notice significant jumps.
1550 Now injecting mix from the dump, slowly in steps. Keeping P1 and P2 between 400 mbar and 450 mbar.
1600 Use tower thermometer as an approximate for H35, which for some reason can not be read out.
1600 1K pot temperature around 1.9 to 2.0 K. still = 2.6 K. MC(Tower) drops from 1.x K.
1610 MC(Tower) = 700 mK, still = 2.48 K, 1K pot = 1.9 K.
1620 MC(Tower) = 632 mK, still = 2.07 K, 1K pot = 1.97 K. liquid hitting the still?
1635 MC(Tower) = 250 mK, still = 2.00 K, 1K pot = 1.93 K. still temp doesn't drop??
1640 MC(Tower) = 200 mK, still = 1.91 K, 1K pot = 1.94 K.
1640 Can we get to base????
1645 MC(Tower) = 190 mK, still = 1.96 K, 1K pot = 1.96 K.
2020 Summary: Found out 1e-4 leak rate from the IVC. Still won't go below 1.8 K while pressure gauge maxed out (>2000 mTorr). Collect mix. stop 1K pot pumping.
TODO

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