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2025/06/30 (Monday)

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  • Lab in-personnel: Himangshu, Yan
Status Run 83 ended. Himangshu back from leave. Evaluating Status for 1K pot test
1000 Turbo pump is turned off, switch is off. Valve on top of pump closed so IVC is still in vacuum. Switch on Turbo pump
1030 Remember that gauge reading is on top of pump Tee now, not underneath the Tee. So connecting scroll to Tee and pump the volume out to get to vacuum
1040 Gauge reading : 1.2e-4 mbar and going down. Turbo pump is working fine .
Lead sheets need to be removed or wrapped with plastic in Room 53. Mike said he can help if not on Tue or Thusrday
1048 The Tee leak is quite more than earlier seen. Pressure gauge reading jumped from 4.6e-4 to 8.6e-3 in about a minute. That's more than the about the time needed to add He during exchange gas step. We might be adding more air than expected through this leak, which might be a cause of frequent clogs in the later cooldown steps
1055 Turning off Turbo and undo the whole Tee structure to apply vacuum grease to all four o-rings
1151 Cleaner all 4 o-rings with ISO and then applied vacuum grease. Rechecked with turbo, leak is still quite high (e-4 to e-2 in 16 seconds) . Attaching Leak detector to point out which o-ring is leaky
1335 Leak checking Tee: Initial Gauge Pressure: 1.9e-4 mbar, At 1 min 50 sec, Pressure: 1e-3 mbar, At 3 min 17 sec, 1.9e-3 mbar, At 4 min 52 sec, Pressure: 3.0e-3 mbar. The only change is the connection to the leak detector line(replaced blank with leak detector bellow).
1409 Pump out 1K pot with scroll pump. With needle valve completely closed, close off pump and see how fast pressure rises:
minutes mbar (P2)
0 8e-2
0.5 2e-1
0.75 3e-1
1.0 3.8e-1
1.25 4e-1
1.5 4.5e-1
1.75 5.2e-1
2.0 6e-1
2.5 6.7e-1
3.0 8e-1
1439 Try another test to see how fast the 1K Pot pressure rises when the pump is closed off, but this time with needle valve open 5 full rotations:
1500 Steps: Keep Main bath valve closed, MB at atm pressure. Open 1K speedivalve to pump out. Open needle valve 5 full rotations. Close scroll pump valve. Within <30 seconds, P2 went off-scale, G3 is at 300 mbar
With the scroll pump valve open, we start the needle valve 0.25 turns at a time
turns mbar (P2)
0 0.1
0.25 0.6
0.5 1.7
0.75 3.0
1.0 3.5
1.5 5
2.0 5
3.0 5.5
4.0 5.5
5.0 5.5
1506 This tells us that there is no blockage on the connection through the needle valve at room temperature. I recall that doing the similar test during cooldown, I was trying to pump on the 1K with needle valve open wide and I donot see any change in pressure on P2, which indicates that there was a blockage at He4 temperatures.

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