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2023/05/05 (Friday)

Previous Day

  • Lab in-personnel: Zach, Himangshu
Status Mixture in fridge, turbo pumping on IVC, fridge cooling slowly
Again yesterday before leaving P2 was creeping up, now it is maxed out at 1000 mbar, maybe there is a small leak somewhere?
1224 MC(Cernox) = 26.5 K, G2/G1 = 521/564 mbar, MB = 1.4 %.
1225 turbo on IVC = 0.19 ubar, after being valved out for a min IVC = 1.4 ubar
1237 Begin LHe transfer @ MB = 1.0 %
1240 Fill LN2 cold trap bath from bomb dewar via 5L dewar
1247 Pause LHe transfer by lifting up transfer lines above liquid level and turning off heater, Himangshu wants to add exchange gas while the MB level is low, reads -0.9% right now
1256 Added 30 ubar of He exchange gas.
1259 MC(Cernox)/Sorb/1K Pot = 14/14/6.99 K, IVC = 22 μbar, G1(fridge) = 549 mbar. G3(MB) = 120 mbar+1atm, MB = -1%
1301 MC temp hit 10 K, open turbo to IVC. IVC pressure hit 4e-4 mbar after about a minute.
1312 Resume LHe transfer
1318 Pump out line leading to 1K Pot with scroll pump (V4a open, 1kpot speedivalve closed). Then switch the line over to the 4He pump. Turn on 4He pump and make sure the pump exhaust is connected to recovery and open valve to recovery lines.
1323 Check pressure in 1K Pot by opening the 1kpot speedivalve with V4a closed: Mechanical gauge = 0.27 bar.
1324 Pump out 1K Pot by slowly opening V4a then the manual valve at the 4He pump until it just starts to make noise, once it quiets down somewhat open it up a little more. continue this until the valve is fully open.
1330 MC(Cernox)/Sorb/MC(H35) = 4.37/4.0/4.35, 1K Pot = 3.13 K / 0.95 mbar. G1 (fridge+dump) = 413 mbar. MB = 57.9%
Leaving mixture in the fridge when starting 1K pot
1333 Open 1K Pot needle valve → 15° (half unit on the needle marks). 1K Pot → 2.84 K / 4.5 mbar.
1340 Open 1K Pot needle valve → 30°. 1K Pot → 2.44 K / 11 mbar.
Since cleaning the needle valve and re-inserting it the new marks could yield slight different results from the old marks
1341 MC(H35) temp starts to decrease quickly, flattens at around 3 K
1346 MC(Cernox)/Still/MC(H35) = 3.03/2.91/3.06, 1K Pot = 2.37 K / 11 mbar. G1 (fridge+dump) = 307 mbar.
1350 Open 1K Pot needle valve → 45°. 1K Pot → 1.90 K / 24 mbar.
1356 Ended LHe transfer @ MB = 94.7 %
1441 MC(H35)/Still/1KPot = 1.86/1.89/1.60 K / 19 mbar, G1(fridge+dump) = 46.2 mbar
1451 Close V3 and V9, leaving 44.9 mbar in the dump. Turn on 3He pump.
1456 Start circulation through Trap 1. V6 → 12.6%. Condenser(G1) peaks at 187.3 mbar. P2 jumps up to 60 mbar, settling down to 50 mbar
1502 V6 → 13.0%. Condenser(G1) peaks at 88.4 mbar. MC(H35) → 0.88 K. Still(P1) → 1.11 K / 3 mbar. After some time the Condenser peaked even higher. Condenser(G1) peaks at 100 mbar
1520 V6 → 13.4%. Condenser(G1) peaks at 101.5 mbar. MC(H35) → 0.56 K. Still(P1) → 1.14 K / 2.2 mbar. P2 = 19 mbar
1523 V6 → 13.8%. Condenser(G1) peaks at 102.7 mbar. MC(H35) → 0.50 K. Still(P1) → 1.13 K / 1.5 mbar.
1528 V6 → 14.4%. Condenser(G1) peaks at 102.6 mbar. MC(H35) → 0.40 K. Still(P1) → 1.12 K / 0.9 mbar.
1530 V6 → 15.0%. Condenser(G1) peaks at 101.1 mbar. MC(H35) → 0.30 K. Still(P1) → 1.11 K / 0.65 mbar.
1533 V6 → 100.%. Condenser(G1) peaks at 101.5 mbar. MC(H35) → 0.24 K. Still(P1) → 1.09 K / 0.32 mbar.
1535 MC(H35) = 158 mK, Still = 1.06 K /0.180 mbar, 1KPot = 1.602 K / 19 mbar, G1/G2 = 97.3/107.5 mbar
1615 Tower(U28)/MC(H35)/Coldplate = 101.0/35.4/141 mK, Still(P1) = 1.10 K / 0.11 mbar / 0 mW, G1/G2 = 68.8/76.7 mbar, 1K Pot(P2) = 45° / 1.606 K / 18 mbar, MB = 93.2%
1617 Open V14 to let the remaining mix out of the dump and into circulation. P1(Still) peaks at 50 mbar then falls again. MC(H35) peaks at 77 mK. Condenser peaks at 95.3 mbar.
1641 Still (P1) < 1 mbar, close V14
1720 Tower(RoX)/Tower(U28)/MC(H35)/Coldplate = 27.2/89.0/30.5/140 mK, Still(P1) = 1.1 K / 0.11 mbar / 0 mW, G1/G2 = 66.0/75.9 mbar, 1K Pot(P2) = 35° / 1.60 K / 18 mbar, MB = 92.3%

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