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2023/02/03 (Friday)

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  • Lab in-personnel: Zach
Status Run 77 beginning, initial LHe transfer yesterday, mixture in fridge with 3He pump off
1200 MC(Cernox)/Sorb/1K Pot = 4.74/8.7/6.8 K, G1/G2 = 544/479 mbar, MB = 43.9%
Yesterday before leaving P2 was creeping up, now it is maxed out at 1000 mbar, maybe there is a small leak somewhere?
1205 Turbo on IVC = 1.2 nbar. With Turbo valve out for 1 minute IVC = 14 nbar
1208 Fill LN2 cold trap bath
1240 Pump out line leading to 1K Pot with scroll pump (V4a open, 1kpot speedivalve closed). Then switch the line over to the 4He pump. Turn on 4He pump and make sure the pump exhaust is connected to recovery and open valve to recovery lines.
1251 After pumping out the lines, closing V4a caused P2 to rise to 5 mbar, why? Open up the 4He pump inlet valve to pump it out again with V4a closed
1254 Check pressure in 1K Pot by opening the 1kpot speedivalve with V4a closed: Mechanical gauge = 0.32 bar.
1256 Pump out 1K Pot by slowly opening V4a then the manual valve at the 4He pump until it just starts to make noise, once it quiets down somewhat open it up a little more. continue this until the valve is fully open.
P2 read max at 1000 mbar after opening V4a (Corrected from previously stated as V1a). Opened the 4He pump valve until it was making a slight noise and P2 went down quickly, to 1 mbar, lower than normal, then I opened the valve all the way and no noise. Why is nothing making sense today?
1300 MC(Cernox)/Sorb/MC(H35) = 4.73/4.2/4.73, 1K Pot = 3.39 K / 1.0 mbar. G1 (fridge+dump) = 525 mbar.
Leaving mixture in the fridge when starting 1K pot
1313 Open 1K Pot needle valve → 15° (half unit on the needle marks). 1K Pot → 2.88 K / 7 mbar.
1317 Open 1K Pot needle valve → 30°. 1K Pot → 2.25 K / 28 mbar.
1320 MC(H35) temp starts to decrease, flattens at around 3 K
1325 MC(Cernox)/Sorb/MC(H35) = 2.97/4.0/2.92, 1K Pot = 2.02 K / 28 mbar. G1 (fridge+dump) = 301 mbar.
1340 MC(H35)/Still/1KPot = 2.36/2.21/1.65 K / 22 mbar, G1(fridge+dump) = 99 mbar
1345 Try the new RoX thermometer, Tower(RoX) = 2.09K, back to the H35 = 2.16 K
1350 1KPot = 12 mbar now, Open 1K Pot needle valve → 37°, no noticeable change.
1352 MC(H35) flattening at 2.11K, must be lambda point, Tower(RoX) = 1.99K, Tower(U28) = 2.05
1355 1KPot = 9,5 mbar now, Open 1K Pot needle valve → 45°, 1K Pot → 1.58 K / 11 mbar.
1400 P2 jumped up, didn't see how high it went, now is at 45mbar, close 1kpot needle valve by 15°, P2 drops to 17 mbar, 1kpot = 1.67 K
P2 oscillating somewhat with needle valve at 30°
1407 P2 somewhat stable at 28 mbar again
1433 Start LHe transfer @ MB = 39.7%
1437 MC(H35)/Still/1KPot = 1.89/1.93/1.66 K / 30 mbar, G1(fridge+dump) = 50 mbar
1442 Close V3 and V9, leaving 28.8 mbar in the dump. Turn on 3He pump.
1445 Start circulation through Trap 1. V6 → 12.6%. P2 jumps up to max, stop circulation
1447 P2 now settled at 9.5 mbar. start circulation through Trap 1. V6 → 12.6%. Condenser peaks at 118 mbar. MC(H35) → 1.42 K. 1kpot goes up to 34 mbar, then recovers to 24 mbar. P1 (still) → 20 mbar.
1453 V6 → 13.0%. Condenser(G1) peaks at 99 mbar. MC(H35) → 1.14 K. Still(P1) → 1.18 K / 5 mbar.
MC(H35) flattens for a bit at 1.05K
1457 V6 → 13.4%. Condenser(G1) peaks at 101 mbar. MC(H35) → 1.07 K. Still(P1) → 1.14 K / 3.4 mbar.
1500 V6 → 13.8%. Condenser(G1) peaks at 108 mbar. MC(H35) → 0.86 K. Still(P1) → 1.11 K / 2.2 mbar.
1504 V6 → 14.4%. Condenser(G1) peaks at 109 mbar. MC(H35) → 0.72 K. Still(P1) → 1.09 K / 1.2 mbar.
1508 V6 → 15.0%. Condenser(G1) peaks at 108 mbar. MC(H35) → 0.47 K. Still(P1) → 1.08 K / 0.7 mbar.
1512 V6 → 100.%. Condenser(G1) peaks at 103 mbar. MC(H35) → 0.29 K. Still(P1) → 1.03 K / 0.24 mbar.
1515 Open 1K Pot needle valve → 37°. 1K Pot = 1.65 K / 38 mbar.
1527 Open 1K Pot needle valve → 45°. 1K Pot = 1.67 K / 45 mbar.
1530 MC(H35) = 41 mK, Still = 1.08 K /0.120 mbar, 1KPot = 1.67 K / 40 mbar, G1/G2 = 82/73 mbar
1531 Tower(U28) = 69.7 mK, Tower(RoX) = 82.3 mK
1535 Open V14 to let the remaining mix out of the dump and into circulation. P1(Still) peaks at 75 mbar then falls again. MC(H35) peaks at 83 mK. Condenser peaks at 109 mbar.
1555 Tower(RoX)/Tower(U28)/MC(H35)/Coldplate = 76.7/61.0/43.8/150 mK, Still(P1) = 1.09 K / 1.8 mbar / 0 mW, G1/G2 = 61.7/58.8 mbar, 1K Pot(P2) = 45° / 1.66 K / 38 mbar, MB = 92.1%
1600 Still (P1) < 1 mbar, close V14
1607 Decrease the 1K Pot needle valve → 35°, P2 → 24 mbar, 1kpot = 1.62K
1631 Tower(RoX)/Tower(U28)/MC(H35)/Coldplate = 70.0/54.0/30.9/145 mK, Still(P1) = 1.09 K / 0.11 mbar / 0 mW, G1/G2 = 70.0/60.5 mbar, 1K Pot(P2) = 35° / 1.62 K / 24 mbar, MB = 91.1%
1647 Tower(RoX)/Tower(U28)/MC(H35)/Coldplate = 70.0/53.7/30.7/145 mK, Still(P1) = 1.09 K / 0.11 mbar / 0 mW, G1/G2 = 70.0/61.0 mbar, 1K Pot(P2) = 35° / 1.62 K / 24 mbar, MB = 91.0%

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