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2018/05/22 (Tuesday)

Previous Day

Status: Replaced 1K pot shaft orings. Pumping on IVC over the weekend.
0819 IVC pumping pressure = 7.4 nbar
0820 Fill LN2 cold trap.
1454 Stop pumping on IVC. IVC pressure = 86 nbar
1459 Let 4.6 mbar He exchange gas into IVC
Cryocleaning mixture
0837 Start cleaning mixture through cold LN2 Trap 2, V6 = 12.4%
0840 Increase V6 to 12.8% to speed up circulation
0854 Increase V6 to 13.0% to speed up circulation
0856 Increase V6 to 13.1% to speed up circulation
0927 Stop cryocleaning, Trap 2 50 minutes.
1030 Start cleaning mixture through cold LN2 Trap 1, V6 = 13.2% Later realized I never opened trap speedivalve.
1038 G2 goes to 950 mbar. This is too aggressive. Close V13A, V14 and open V9 to let some back into the dump.
1039 Reduce V6 to 13.0%. Once G2 falls to 650 mbar, close V9 and reopen V14 and V13A to restore flow at safe pressures.
1045 G2 is slowly climbing again to 800 mbar instead of falling like normal. Maybe this trap is full and getting clogged up? Reduce V6 again to 12.9%
1047 We still have flow, but it seems less than normal.
1120 Stop cryocleaning, Trap 1 50 minutes.
1133 Crap, realize that I had forgotten to open the speedivalve to trap 1 in this last “cleaning”. That's why things were strange. Not sure why it seemed like I had flow though. Continue pumping mix to dump.
1138 Restart cleaning mixture through cold LN2 Trap 1, V6 = 13%
1040 Increase V6 to 13.1% to speed up circulation
1143 Increase V6 to 13.2% to speed up circulation
1145 Increase V6 to 13.3% to speed up circulation
1228 Stop cryocleaning, Trap 1 50 minutes.
1321 Check pressure in warm Trap 2: 7.5 mbar. Pump out with scroll pump
1334 Start cleaning mixture through cold LN2 Trap 2, V6 = 12.8%
1337 Increase V6 to 12.9% to speed up circulation
1339 Increase V6 to 13.0% to speed up circulation
1347 Increase V6 to 13.1% to speed up circulation
1424 Stop cryocleaning, Trap 2 50 minutes.
1438 Check pressure in warm Trap 1: 17.5 mbar. Pump out with scroll pump
1445 Start cleaning mixture through cold LN2 Trap 1, V6 = 13.2%
1450 Increase V6 to 13.3% to speed up circulation
1455 Increase V6 to 13.4% to speed up circulation
1505 Increase V6 to 13.5% to speed up circulation
1535 Stop cryocleaning, Trap 1 50 minutes.
1550 Check pressure in warm Trap 2: 130.8 mbar. Dump pressure is still at 720 mbar, so we must have got some air in while moving the traps around. Dang! Pump out with scroll pump.
1600 Tighten LN2 cold trap o-ring seals slightly, though they seem pretty secure. We'll just try again tomorrow…

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