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2016/06/02 (Thursday)

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Status: Fridge cooling toward 4K overnight. Turbo-pumping IVC overnight. Trap 1 at room temperature overnight.
0800 MC(Cernox) = 24.9 K, Sorb = 20 K, IVC = 8.6e-7 mbar pumping, 4.6e-6 mbar with pump valved out. Isolate IVC.
0810 Trap 1 reached 5 mbar on P2. Pump out Trap 1.
0815 Put LN2 Cold Trap 1 bath and fill bath. Trap 2 is also clean and in bath.
0820 Tower = 25.7 K, MC(H35) = 19.6 K, Still = 18.4 K, Coldplate = 37.0 K, MC sensor = 2.332 kΩ (no calibrated reading on vi), 1K Pot > 7 K
0830 Open 1K Pot needle valve 90 degrees. No response in Sorb or 1K Pot temperatures
0840 Pump out lines leading to 1K Pot, then isolate pump. Close needle valve then open 1K Pot speedivalve - pressure on mechanical gauge on 1K Pot pumping line rises to about 1/4 bar. Open needle valve until this rises again, over 90 degrees. Sorb and 1K Pot temperatures fall quickly as pot fills with LHe. Pressure rises to 136 mbar relative on G3 (MB overpressure).
0842 Sorb = 5.3 K, 1K Pot = 4.1 K
0845 Let mixture through cold trap into fridge, through V9 (3He pump is off), V13a, Trap 1 speedivalve (V12a closed), V1, and condenser valve.
0850 Still = 16.3 K and falling.
0900 Sorb/1K Pot/Still/Coldplate/MC(Cernox)/Tower = 5.4/4.2/14.3/37/24.5/25.4 K. So Still is cooling significantly, CP/MC/Tower down slightly.
0905 G1/G2 (Condenser/Trap) = 670/645 mbar. G1 is still rising, G2 is still falling.
0910 Close V13a to leave some mixture in the dump. G1(Condenser) = 700 mbar, G2(Dump) = 644 mbar
0915 Set 1K Pot needle valve to about 50 degrees. Start pumping on 1K Pot with 4He pump. Opening and closing V4a so as not to put too much strain on pump. Open 4He Pump exhaust to recovery.
0920 Close 1K Pot needle valve completely, then leave V4a open to pump on pot. Trying to be a little more gentle.
0925 Sorb = 4K (minimum?), 1K Pot = 1.6 K / 8.0 mbar, Still = 4.2 K, Condenser pressure falling, now at 234 mbar.
0930 1K Pot fell to < 1 mbar. Open 1K Pot needle valve to 45 degrees. 1K Pot → 1.7 K / 36 mbar.
0932 Open V13a to let more mix into fridge. Monitoring 1K Pot pressure. It doesn't go up much (50 mbar).
0935 Open V12a to 1.5% - now G1 starts to rise, 1K Pot pressure rises to 400 mbar. Close V13a. Begin letting mix in through V13a in controlled fashion to regulate 1K Pot pressure.
0940 On 5th cycle pot pressure stops increasing. Leave V13a open to let mixture into condenser.
0945 Still/Coldplate/MC(Cernox)/Tower = 4.3/35/24.1/24.9 K. CP/MC/Tower cooling slowly.
0945 1K Pot = 1.7 K / 60 mbar. G1/G2 = 490/490 mbar and falling steadily. Open V12a completely. Causes brief surge in condenser and 1K Pot pressures.
1000 1K Pot = 1.8 K / 75 mbar, oscillating. G1/G2 = 440/400 mbar. Close 1K Pot needle valve 5 degrees narrower. Oscillations calm down.
1005 Still/Coldplate/MC(Cernox)/Tower = 3.8/31/23.6/24.4 K
1015 1K Pot = 1.7 K / 38 mbar, oscillating slightly. G1/G2 = 375/340 mbar.
1015 Open Still gate valve. Causes a surge in 1K Pot temperature. This is somehow a result of the sudden decrease in pressure on the still side. MC temperature decreases a little more rapidly. 1K Pot temperature settles back after 5 minutes. 1K Pot pressure is now more stable.
1020 Still/Coldplate/MC(Cernox)/Tower = 3.6/27/23.1/23.8 K
1025 1K Pot = 1.7 K / 40 mbar. G1/G2 = 400/360 mbar and falling slowly.
1030 Close V9 leaving 356 mbar in dump. Then turn on 3He pump, which pushes mixture from back of pump into condenser. Surge in 1K pot temperature and pressure and G1/G2, also brief decrease in Still temperature. Then things stabilize quickly.
1035 1K Pot = 1.7 K / 40 mbar. G1/G2 = 350/320 mbar and falling.
1040 Start circulation. At V6 = 13% response seen - 1K Pot surge to 2.2 K / 240 mbar, circulation pressures rise from 300 to 500 mbar, Still temperature falls a little.
1045 Circulation pressures falling again, G1/G2 = 400/380 mbar. 1K Pot = 2.1 K / 40 mbar, temperature slowly falling. Still temperature flat at 3.1 K. Start opening V6 more in increments of a few tenths of a percent.
1050 Still/Coldplate/MC(Cernox)/Tower = 2.9/26/21.1/21.9 K
1055 At V6 = 13.3%, circulation pressures started climbing steadily and didn't fall. At close to 1 bar, stop circulation by closing V6 to 12%. Circulation pressures falling again.
1100 Start circulation again with V6 = 13.2%. Circulation pressures stabilize at around 600 mbar. Still at around 3.1 K.
1120 1K Pot = 2.1 K / 38 mbar, temperature falling. G1/G2 = 330/325 mbar and falling.
1145 Still/Coldplate/MC(Cernox)/Tower = 2.5/18/18.9/19.3 K
1150 1K Pot = 1.7 K / 22 mbar. G1/G2 = 135/125 mbar. All quite stable.
1155 Increase V6 to 13.5%. 1K Pot and circulation surge but come back down and stabilize quickly.
1210 Still/Coldplate/MC(Cernox)/Tower = 2.1/21/17.5/17.9 K
1215 Increase V6 to 14.0%
1225 Circulation pressures running away again, reduce V6 to 13.0%. Pressures begin to fall.
1245 After a few minutes pressures increased again and hit 1 bar. Closed V6 to 10% and opened V9 to release pressure into dump.
1255 MC fall quickly to below 4 K
1300 Close V9 again isolating 373 mbar of mixture in dump.
1305 Still/Coldplate/MC(Cernox)/Tower = 2.5/3.6/3.1/4.9 K. G1/G2 = 200/185 mbar and falling.
1310 Start circulation again, V6 = 13.2%
1315 Increase V6 to 13.5% because circulation pressure still falling. Still → 1.8 K
1325 Still down to 1.6 K, starting to level out. G1/G2 = 105/120 and level. Increase V6 to 13.7%.
1336 P1 (Still) pressure falls into readable range
1355 Still = 1.47 K / 400 mbar, Coldplate/MC(Cernox)/Tower = 1.9/6.6/7.1 K (MC and Tower higher??) G1/G2 = 125/140 mbar. 1K Pot = 1.7 K /36 mbar
1400 V6 → 14%. Still pressure falls a lot, Still temperature decreases a bit, 1K Pot and circulation pressures not affected much.
1405 V6 → 14.5%. Still → 1.19 K / 4 mbar
1406 Surge in Still/Circulation/1K Pot to 1000/450/230 mbar, then back down.
1410 Still = 1.49 K / 22 mbar, Coldplate/MC(Cernox)/Tower = 1.8/2.6/4.5 K (MC and Tower much lower), G1/G2 = 140/170 mbar and falling. 1K Pot = 1.6 K /28 mbar and falling.
1415 V6 → 15%. There are oscillations in MC temperature and circulation pressure, possibly superfluid/normal fluid transition forming.
1435 V6 → 100%. Still = 0.60 mbar. MC(H35) = 1.2 K
1440 Some oscillations in MC temperature and Still pressure. MC not going any lower than 1.2 K.
1445 Begin opening and closing V14 to let more mix from dump into circulation. Throttle to prevent circulation pressures from going too high.
1510 MC = 1.25 K, not falling. Tower = 3.6 K. I'm concerned that this tower has a thermal short between 4K stage and other stages…
1515 Still = 1.33 K / 1.2 mbar, Coldplate/MC(H35)/Tower = 1.5/1.4/3.6 K, G1/G2 = 600/580 mbar and creeping up. 1K Pot = 1.75 K / 45 mbar and falling.
1535 1K Pot pressure, circulation pressure, and still pressure are all oscillating in phase. Something is producing a strain on the fridge.
1540 Switch to one-shot mode, close V13a and open V9. Circulation pressures keep creeping up, can't maintain this.
1515 Still = 1.14 K / 0.22 mbar, Coldplate/MC(H35)/Tower = 1.5/1.3/3.4 K, G1/G2 = 24/373 mbar. 1K Pot = 1.6 K / 6 mbar.
1555 Still = 1.14 K / 0.14 mbar, Coldplate/MC(H35)/Tower = 1.4/1.2/3.25 K, G1/G2 = 8/420 mbar. 1K Pot = 1.7 K / 22 mbar.
1620 Still = 1.20 K / 0.09 mbar, Coldplate/MC(H35)/Tower = 1.4/1.2/3.0 K, G1/G2 = 3/505 mbar. 1K Pot = 1.7 K / 32 mbar.
1635 Close V6 to end the one-shot, open V13a to let mixture back into fridge.
1640 Turn off 3He pump
1730 Fill LN2 cold trap full.

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