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2014/01/27

1450 Fill LN2 cold trap full.
1620 Interrupt cryocleaning to commence pumping mixture to the dump.
1725 Initial throughput test gives throughput rate of roughly 7 mbar/min. This is much less than the expected rate of ~45 mbar/min.
1805 Throughput test Berkeley-style yields values listed in Tables 1 & 2. This is lower than that in test during a previous run (2013/10/26).
It is possible that poor throughput is due to higher mixing chamber temperature of 93-97 K during these tests. As we do not have any phonon channels on this crystal, it may be worth cooling down to liquid helium temperatures to determine what sort of base temperature we hit.
Table 1: Berkeley-Style Throughput Test 1 Results.
Time [s] P1 [μbar] G1 [± 1 mbar] G2 [± 1 mbar]
0 14 ± 0.5 677 609
20 15 ± 0.5 670 602
40 18 ± 0.5 671 602
60 38 ± 1 671 601
80 85 ± 2.5 671 601
100 160 ± 5 671 600
120 220 ± 5 671 600
140 300 ± 10 670 600
160 360 ± 10 670 599
180 400 ± 25 670 599
200 450 ± 25 670 599
220 550 ± 25 670 598
240 650 ± 25 670 598
260 750 ± 25 670 597
280 850 ± 25 670 597
300 950 ± 25 670 597
Table 1: Berkeley-Style Throughput Test 2 Results.
Time [s] P1 [μbar] G1 [± 1 mbar] G2 [± 1 mbar]
0 17 ± 0.5 678 609
20 17 ± 0.5 671 602
40 20 ± 0.5 671 602
60 40 ± 1 671 601
80 90 ± 2.5 671 601
100 160 ± 5 671 600
120 220 ± 5 671 600
140 300 ± 10 671 599
160 360 ± 10 671 599
180 400 ± 25 671 598
200 450 ± 25 671 598
220 550 ± 25 671 598
240 650 ± 25 671 597
260 700 ± 25 671 597
280 850 ± 25 671 597
300 950 ± 25 671 597
1845 Having recovered mixture (653 mbar - appears as though we lost some due to our leaky circulation pump last run), close gate valve and condenser line speedivalve to isolate fridge. Close all valves on IGH except V9.
Noticed that stopper had popped out from port into main bath at top of fridge. Port lies next to that used for transfer sticks. Probably popped out due to relatively high main bath pressure. Not sure when this occurred, and air may have leaked in. Evacuate main bath, and pressure drops below 0.5 mbar, indicating that there is probably no condensed water vapour inside main bath. Probably safe to commence transfer. Overpressurise main bath with He-4 gas.
1900 Fill IVC with 0.046 mbar He-4 exchange gas. Commence helium transfer.