UMN CDMS Wiki archive
start › cdms › k100 › run_diary › 20200820

2020/08/20 (Thursday)

Previous Day

  • Lab in-person: Matt
  • Virtual partner: Michael, Zach
Setup Run 73. DIB 1/3/4 → Stripline 43/48/41 → pi-filters 1/2/3 → Cable 3/1/2 → nothing/nothing/accessory_interposer → HV_Conn 1/3/2 → HV 1/2 → DCRCX(4)/DCRC55(1)-master; DCRC33(2) → HV control. DCRCs off overnight. Lead/poly shield erected (4 lead walls, 2 poly walls).
Status: Added more 4He to the mixture three days ago, fridge couldn't cool below 0.4 K. Yesterday boiled off bath and warmed fridge to 12 K to pump out helium from IVC, then transferred LHe. Will try 1K Pot and circulation today.
0835 Matt Fritts body temperature 97.7 °F
0900 Matt enters lab
0915 MC(Cernox)/Sorb/1K Pot = 5.2/7.5/5.9 K, Turbo on IVC = 4.0 nbar, G1(fridge) = 575 mbar (3He pump on). G3(MB) = 136 mbar+1atm.
1010 Pump out line leading to 1K Pot Speedivalve using 4He pump.
1015 Check pressure in 1K Pot: 12/30 = 0.4 atm on mechanical gauge. 1K Pot temperature dips to 3.6 K.
1025 Pump out 1K Pot in steps, alternating between V4a and the 1K Pot speedivalve, opening V4a for short bursts to keep P2 below about 10 mbar. After several iterations leave V4a and 1K Pot speedivalve open. 1K Pot → 3.3 K / 3.2 mbar
1030 MC(H35)/Tower = 5.16/5.12 K. Sorb = 4.1 K. G1(Fridge) = 507 mbar and falling.
1035 MC(H35) falls quickly to 3.5 K then settles.
1035 Open 1K Pot needle valve → 10°. 1K Pot → 3.1 K / 4.0 mbar.
1040 Open 1K Pot needle valve → 20°. 1K Pot → 2.8 K / 8.0 mbar. MC(H35) = 3.41 K, G1(fridge) = 450 mbar, falling faster.
Open 1K Pot needle valve → 30°. 1K Pot → 2.4 K / 16.0 mbar.
1045 Open 1K Pot needle valve → 40°. 1K Pot → 2.0 K / 30.0 mbar, with some oscillations. MC(H35) = 3.19 K, G1(fridge) = 347 mbar. Sorb = 4.0 K.
1055 Fill LN2 cold trap bath
1112 Begin LHe transfer @ MB = 67.2%
1115 1K Pot pressure has dropped a lot. 1K Pot = 1.53 K, 7.5 mbar.
Open 1K Pot needle valve → 50°. 1K Pot → 1.57 K / 12.0 mbar. MC(H35) = 2.13 K, G1(fridge) = 62 mbar.
1120 Open 1K Pot needle valve → 60°. 1K Pot pressure increases slowly, then shoots off scale, then falls again. This happened last time too at about the same MC temperature - close to the lambda point for superfluid He transition. MC(H35) = 2.12 K
1130 1K Pot = 1.74 K / 450±50 mbar. Close needle valve → 50°.
1131 End LHe transfer @ MB = 92.3%
1155 1K Pot = 1.69 K / 57±2 mbar. MC(H35) = 2.09 K, cooling very slowly. G1(Fridge) = 56 mbar, was flat but now falling.
1205 Matt leaves lab
1230 MC(H35) suddenly drops, 2.08→1.97 K, then starts cooling steadily. G1(Fridge) suddenly rises at the same time, 48.5→51.5 mbar, then starts falling at same rate as before.
1245 1K Pot = 1.69 K / 60±2 mbar. MC(H35) = 1.88 K, G1 (fridge) = 49 mbar.
1245 Close V3 and V9, leaving 48 mbar (G2) in the dump. 3He pump is on.
1250 Start circulation through Trap 1. V6 → 12.8%. Condenser peaks at 122 mbar. MC falls to 1.68 K. 1K Pot pressure spikes for a moment.
Note that G2 peaks higher than G1, that's unusual. Is the LN2 Trap clogged from dirty mixture?
1255 V6 → 13.2%. Condenser peaks at 117 mbar. MC(H35) → 1.61 K
1303 V6 → 13.4%. Condenser peaks at 120 mbar. MC(H35) → 1.53 K
1310 V6 → 13.6%. Condenser peaks at 128 mbar. MC(H35) → 1.49 K. Still → 100 mbar.
1315 V6 → 14.0%. Condenser peaks at 145 mbar. MC(H35) → 1.28 K. Still → 9 mbar.
1320 MC falls to 1.13 K then starts rising, Still and Condenser pressures rise too, looks like we're pushing into the Al Tc. MC peaks at 1.21 K then falls.
1320 V6 → 14.4%. Condenser peaks at 130 mbar. MC(H35) → 1.05 K. Still → 4.0 mbar.
1325 MC changed slope a few times but never rose again, now 0.91 K. Sorta looks like now that we have more mixture it has more cooling power, pushes fridge below the Al Tc more easily.
1330 V6 → 15.0%. Condenser peaks at 147 mbar. MC(H35) → 0.72 K. Still → 2.2 mbar.
1340 V6 → 100%. Condenser peaks at 145 mbar. MC(H35) → 0.20 K. Still → 0.240 mbar.
1350 MC(H35) = 57 mK, Still = 0.130 mbar, G1/G2 = 106/116 mbar. Looking good! MC continues to cool.
1405 MC(H35) = 41.6 mK, Still = 0.095 mbar, G1/G2 = 89/99 mbar.
1420 MC(H35) = 32.8 mK, Still = 0.095 mbar, G1/G2 = 94/102 mbar.
1420 Open V14 to let the remaining mix out of the dump and into circulation. P1(Still) peaks at 50 mbar then falls again. Condenser peaks at 140 mbar. MC(H35) peaks at 80 mK. 1K Pot pressure reacts very slightly.
1445 MC(H35) = 33.4 mK, Still = 0.75 mbar, G1/G2 = 98/105 mbar.
1445 Close V14
1455 MC(H35) = 29.8 mK, Still = 0.110 mbar, G1/G2 = 99/106 mbar.
1540 MC(H35) = 28.8 mK, Still = 0.095 mbar, G1/G2 = 102/109 mbar. 1K Pot = 1.70 K / 55±2 mbar
MC is cooler than it was the first time we cooled down, that's nice. Seems to have flattened out. Let's try heating the still, for fun.
1540 Turn on Still Heater to 5 mW. G1/G2 rise to 126/134 mbar, Still rises to 0.16 mbar. MC spikes to 31.5 mK, then falls to 29.0 mK, then starts to rise.
1555 MC peaks at 29.5 mK then starts coming down again. Let's see what happens.
1655 MC has settled at 29.0 mK, a little warmer than before the Still heater.
1655 Turn off Still Heater. MC dips all the way down to 27.6 mK but then rises to 28.6 mK, looks like it's settling.
1725 MC(H35) = 28.6 mK, Still = 0.095 mbar, G1/G2 = 111/116 mbar.
1750 MC(H35) = 28.8 mK, Still = 0.095 mbar, G1/G2 = 112/117 mbar. Looks like it's back to where it was before trying the Still Heater.

Next Day