2019/09/30 (Monday)
| Status: Warming up after leak seen from bath to IVC | |
| 1250 | Tried starting Jiajin and power cycling it, pc is not responding, power switch causes momentary blinking that stops after switch is released. |
| 1252 | MC(Cernox) = 124.8 K. Going to start another leak check with MB in same position as previous, though the LN2 has likely boiled off and possibly pushed out the helium. |
| 1255 | Rubber stopper was missing from MB fill port, must have popped of during the weekend, or someone moved it. I found it sitting near the 1k pot needle valve. |
| 1300 | Turn on Leak Detector, IVC = 10 nbar, MC(Cernox) = 124.2 +/- 5 K. |
| 1307 | Leak Detector settles to baseline, Leak Rate = 1.2e-9 mbarL/s, MC(Cernox) = 124.5 K |
| 1309 | Open leak detector to turbo and IVC, Leak Rate = 1.0e-8 mbarL/s, MC(Cernox) = 125.0 K |
| 1311 | Valve off turbo, Leak Rate = 1.45e-7 mbarL/s, MC(Cernox) = 124.9 K |
| 1315 | Leak Rate is low, let's try squirting some He at different the different seals |
| 1319 | No leak response, even squirting directly into the main bath, let's try pumping out the main bath and trying again. |
| 1328 | Begin pumping on MB, hook up scroll pump in the back, open 4a and 1a. |
| 1334 | P2 comes on scale and begins falling |
| 1343 | P2 = 3.2 mbar. |
| 1351 | P2 is stable at 3.0 mbar, stop pumping on the MB. |
| 1354 | Start up Leak Detector, MC(Cernox) = 127 K |
| 1400 | Baseline of leak detector is off scale low, open leak detector to turbo and IVC, Leak Rate = off scale low |
| 1403 | Valve off turbo, Leak Rate = 5.0e-8 mbarL/s, MC(Cernox) = 126.2 K |
| 1405 | Squirt seals to check for leaks |
| 1410 | Still nothing, going to try and flush the MB with He |
| 1415 | Leak rate spikes during He flush, Leak Rate = 7.1e-6 mbarL/s, MC(Cernox) = 125.7 K |
| 1419 | Accidentally disconnect and vent leak detector before reopening the turbo, IVC = 1.9e2 mbar |
| 1420 | Accidentally disconnected scroll pump before spiand vent turbo on nning down leak detector turbo, it quenched. Turn of leak detector, attach scroll pump to IVC to begin pumping down. |
| 1431 | Reopen turbo valve and disconnect scroll pump, IVC = 1e-3 mbar. |
| 1457 | IVC = 74 nbar, begin pumping out MB in preparation for nitrogen flush, MC(Cernox) = 128.5 K |
| 1502 | P2 comes on scale and begins falling. |
| 1515 | Flush main bath with N2. |
| 1520 | Turn on Leak detector and open it to Turbo and IVC, Leak Rate = 4.4e-9 mbarL/s, MC(Cernox) = 129 K |
| 1523 | Valve of turbo, Leak Rate = 1.2e-7 mbarL/s, MC(Cernox) = 128.3 K |
| 1527 | Test squirting He into MB at various heights using LN2 transfer stick. At each height, let in 1 hose length of He at 3.5 psi. Try just below the top of the main, bath, about half the transfer stick length, just above the LHe fill funnel, and fully inserted into the LHe fill funnel. Leak rate never rises above baseline level of 100 pbar L/s. |
| 1548 | Increase He gas pressure to 7 psi and repeat the above test. Just above the transfer cone, rate is flat at about 100 pbar L/s. With transfer stick inserted into cone, rate slowly rises to 118 pbar L/s. Hard to tell, but the leak is probably one of the lower 2 seals on the IVC. |
Warmup
| 1600 | Turn on MC and Still heaters to 20 mW each. |
|---|---|
| 1612 | IVC = 630 nbar. Let He gas into IVC one hose-length at a time until IVC = 0.1 bar. |
| 1640 | Let 8.6 mbar N2 gas into vacuum manifold. Then open cryostat vacuum jacket valve to let this into the vacuum jacket. Vacuum jacket → 300 ubar |