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2019/04/29 (Monday)

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Status Discovered a blockage Friday. Warming up. Mixture has been cleaned 6 times. Left mixture cooling in LN2 Cold Trap 2 over the weekend.
Removed 5.6 mbar
Setup DIB1/3/4 → 3.2 MHz filters 2/3/1 → cable 3/1/2
0855 Turbo on cryostat vacuum jacket = 16 nbar. With pump valved out vacuum jacket = 250 nbar. MC(Cernox) = 290.5 K
0855 DIB4pD SQUID is reading OK, 3.293 kOhm
0900 Pump mixture out of LN2 Cold Trap 2 to dump.
0910 Start cryocleaning mixture through LN2 Cold Trap 1, V6 = 13.1%
0930 Start pumping out IVC with scroll pump. After a couple of minutes switch to turbo pump.
0915 Increase V6 → 13.2% to speed up flow
0940 Increase V6 → 13.3% to speed up flow
1010 Stop cleaning through Trap 1 after 60 min. G2 flow pressure was 580-820 mbar. Pump mixture to dump.
Removed 15.8 mbar. That's significantly higher. Maybe because I circulated at significantly higher pressure?
1020 LN2 Trap 2 is mostly warm. Check contents: 6.9-1.3 = 5.6 mbar on G1. Pump out with scroll pump.
1035 Start cryocleaning mixture through LN2 Cold Trap 2, V6 = 13.0%
1040 Increase V6 → 13.1% to restart flow
1045 Increase V6 → 13.2% to speed up flow
1050 Increase V6 → 13.3% to speed up flow
1135 Stop cleaning through Trap 2 after 60 min. G2 flow pressure was 575-830 mbar. Pump mixture to dump.
Removed 3.9 mbar
1150 LN2 Trap 1 is mostly warm. Check contents: 17.3-1.5 = 15.8 mbar on G1. Pump out with scroll pump.
1210 Start cryocleaning mixture through LN2 Cold Trap 1, V6 = 12.9%
1220 Increase V6 → 13.0% to speed up flow
1245 Increase V6 → 13.1% to speed up flow
1310 Stop cleaning through Trap 1 after 60 min. G2 flow pressure was 580-700 mbar. Pump mixture to dump.
Removed 7.2 mbar
1330 LN2 Trap 2 is mostly warm. Check contents: 5.3-1.4 = 3.9 mbar on G1. Pump out with scroll pump.
1345 Start cryocleaning mixture through LN2 Cold Trap 2, V6 = 12.9%
1405 Increase V6 → 13.1% to speed up flow
1425 Increase V6 → 13.2% to speed up flow
1500 Stop cleaning through Trap 2 after 75 min. G2 flow pressure was 575-620 mbar. Pump mixture to dump.
Removed 4.1 mbar
1520 LN2 Trap 1 is mostly warm. Check contents: 8.7-1.5 = 7.2 mbar on G1. Pump out with scroll pump.
1600 Start cryocleaning mixture through LN2 Cold Trap 1, V6 = 13.0%
1630 Increase V6 → 13.3% to speed up flow
1640 Increase V6 → 13.4% to speed up flow
1650 Stop cleaning through Trap 1 after 50 min. G2 flow pressure was 575-790 mbar. Pump mixture to dump.
Removed 6.5 mbar
1705 LN2 Trap 2 is mostly warm. Check contents: 5.4-1.3 = 4.1 mbar on G1. Pump out with scroll pump.
1710 Close v9 then turn off 3He pump, isolating pump from dump. Open dump through v4 and v12B+speedivalve to cold LN2 Trap 2 to cool overnight.

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