UMN CDMS Wiki archive
start › cdms › k100 › run_diary › 20150402
0825 Fill cold trap with LN
0830 Dump = 806.7 mbar @ G2
MC = 6.72 K. Drifted up from 6.1 K over last 12 hours. Main bath at 71.7%.
Turbo pump pressure reads 1e-8 mbar, both with pump valve open and closed.
0840 Begin cleaning mixture through Trap 2. V6 open 12.8%.
0847 G1/G2 = 690/630 mbar. Increase V6 to 13.2%
0853 Tube from trap a bit frosty, reduce V6 to 13.0 %
0857 MC = 6.75 K (Cernox), Still thermometer = 2.5434 kOhm
0913 G1/G2 = 694/661 mbar
0917 Stop cleaning mixture. Pump mixture to dump.
0937 Dump = 807.5 mbar @ G2
0939 Start 1K Pot
0946 Begin condensing mixture
1016 Open V12 fully. Currently mixing chamber temperature is at 2.5 K, G1=179 mbar, G2=202 mbar, and 1K Pot is at 1.8 K.
1026 With mixing chamber temperature at 2.1 K, G1= 86 mbar, and G2=105 mbar, close V9 and commence circulation procedure.
1036 MC = 1.75 K (H35), Still thermometer = 3.693 kOhm
1058 Open V6 completely. Mixing chamber temperature at 800 mK, G1=132 mbar, G2=164 mbar.
1121 MC = 35.5 mK !! you read that right !! Still = 1.18 K
1126 MC = 31 mK, G1/G2 = 74/89 mbar, Still = 0.095 mbar / 1.17 K, 1K Pot = 1.82 K / 90 mbar
1136 MC = 27 mK
1140 MC = 30 mK
1144 close pot needle valve somewhat
1146 MC = 25 mK, G1/G2 = 67/82 mbar, Still = 0.075 mbar, 1K Pot = 1.73 K / 24 mbar
1152 MC = 24.7 mK, G1/G2 = 59/75 mbar, Still = 0.065 mbar / 1.11 K, 1K Pot = 1.68 K / 12 mbar
1200 MC = 24.3 mK
1201 apply 1 mW to still
1204 MC = 24.2 mK, G1/G2 = 63/78 mbar, Still = 0.080 mbar / 1.11 K, 1K Pot = 1.67 K / 12 mbar
1205 increase still heat to 2 mW
1212 MC = 24.0 mK, G1/G2 = 66/82 mbar, Still = 0.095 mbar
1213 increase still heat to 4 mW. base goes up to 24.2 mK then back down a bit
1218 MC = 24.1 mK, G1/G2 = 69/88 mbar, Still = 0.120 mbar
1221 increase still heat to 8 mW. base rises to 25 mK and flattens
1225 MC = 25.0 mK, G1/G2 = 73/96 mbar, Still = 0.170 mbar
1226 reduce still heat to 2 mW
1259 MC = 24.9 mK. Turn off still heat and prepare to add remaining mixture (about 100 mbar is still in the dump)
Lakeshore bridge settings: range 200 kOhm, excitation 20 uV, power 1.65 fW; voltage mode
1305 MC = 23.8 mK, still = 0.065 mbar. Begin adding more mix through V14
Opened V14 until P1 read 1000 mbar then closed again. MC rose to 52 mK and began dropping again.
G2 rose by 50 mbar while mix was being added. This may be an indication of how much mixture was removed from dump.
1318 MC bottoms out at 26.7 mK. so not as good as before. Actually not bottomed out - starts creeping down again…
1334 MC = 24.4 mK, G1/G2 = 60/74 mbar, Still = 0.100 mbar (0 mW), 1K Pot = 1.67 K / 12 mbar
1356 MC = 23.7 mK, G1/G2 = 59/74 mbar, Still = 0.100 mbar (0 mW), 1K Pot = 1.67 K / 12 mbar
1410 MC = 23.5 mK
1412 apply 2 mW to still. Base goes up to 23.6 mK then back down to 23.5 mK
1420 MC = 23.5 mK, G1/G2 = 66/83 mbar, Still = 0.130 mbar / 2 mW, 1K Pot = 1.67 K / 12 mbar
1430 MC climbs a bit, to 23.7 mK
Opened V14 until P1 read 1000 mbar then closed again. MC rose to 45 mK and began dropping again.
G2 rose by 35 mbar while mix was being added.
1444 MC drops to 25 mK then bounces up a bit, similar pattern to last time we added mix
1447 Letting the rest of the mix in. Leaving V14 open. G2 rose a total of 70 mbar during the process of adding mix.
1451 MC peaks at 116 mK then falls again
1519 P1 at 0.6 mbar, close V16. MC = 29 mK
1525 MC = 27.5 mK, G1/G2 = 61/75 mbar, Still = 0.100 mbar (0 mW), 1K Pot = 1.67 K / 11 mbar
1547 MC = 23.7 mK, G1/G2 = 61/76 mbar, Still = 0.100 mbar (0 mW), 1K Pot = 1.68 K / 12 mbar
1600 MC = 23.5 mK
Note: MC temperatures quoted here are read off the LabVIEW VI, which uses the functional form fit
… the LakeShore Bridge display, based on the raw data, does not exactly agree
… currently for example the LabVIEW reads 23.4 mK, LakeShore reads 23.8 mK
1617 MC = 23.4 mK, G1/G2 = 61/76 mbar, Still = 0.100 mbar (0 mW), 1K Pot = 1.68 K / 12 mbar
1631 MC = 23.3 mK. Fill LN2 cold trap full.
1708 Mixing chamber stable at 23.3 MK, P1=100 ubar, G1=61 mbar, G2= 76 mbar, 1K Pot steady at 1.67 K, and P2=12 mbar. Turn on Still heater to 2 mW.
1940 Mixing chamber temperature has stabilised at 23.5 mK after a couple of oscillations, and has remained at this temperature for a couple of hours. Pressures in P1, G1 & G2 are 140 μbar, 67 mbar & 82 mbar respectively. Temperature of 1 K pot steady at 1.67 K and pressure in P2 is 11 mbar. Turn off still heater. Wait for fridge to recover.
2230 Mixing chamber temperature has stabilised at 23.1 mK. Pressures in P1, G1 & G2 are 100 μbar, 61 mbar & 69 mbar respectively. Temperature of 1 K pot steady at 1.67 K and pressure in P2 is 12 mbar. Commence incrementing power to mixing chamber heater and recording effect on temperature. Start with power of 2 μW.
2355 Mixing chamber temperature appears to have stabilised at 24.9 mK. That took a while. That probably isn't completely unexpected - the fridge appears to be behaving as she should. Turn off mixing chamber heater. We may continue test tomorrow.