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2014/09/01

0405 Fill N2 cold trap full.
Commence cryocleaning mixture through nitrogen cold trap 2. Dump pressure 631 mbar.
0630 Mixing chamber temperature has dropped below 81 mK - good enough. Start pumping exchange gas out of IVC.
1440 Fill N2 cold trap full.
1520 Background helium leak rate 2.6E-9 mbar l/s. Commence nitrogen blow-out.
1615 Helium pressure has dropped. Leak rate increased gradually to 3.3E-7 mbar l/s. Normally, one would call this a gross leak. However, the way the leak rate increased over the course of the blow out wouldn't seem to indicate that it is anything other than background.
1630 Since turning off helium gas, leak rate has increased to 3.6E-6 mbar l/s. Not sure what that means. Start evacuating main bath. Leak rate has started to decrease. Not sure what that means either.
1640 Pressure in main bath <1 mbar: no liquid nitrogen left.
Helium leak rate has dropped to 3.2E-7 mbar l/s, and is continuing to fall very slowly. Time to try filling the main bath with helium.
1650 Overpressurise main bath with helium. Leak rate started to rise immediately. It appears to have plateaued at 4.5E-6 mbar l/s. This is almost certainly a sign of a leak. We should lower the dewar.
1655 Isolate leak checker and leave turbo pump isolated. Pressure in IVC <4.6E-3 mbar (low pressure gauge is faulty). Let's see if IVC pressure increases.
1735 Lower dewar. IVC pressure <4.6E-3 mbar.