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2013/11/22

0045 Interrupt cryocleaning. Pump mixture into dump in preparation for condensation.
IVC pressure 1E-6 mbar. Mixing chamber temperature 11.7 K and falling slowly. Mixing chamber temperature was rising for a couple of hours, before starting to fall again over the last hour. I don't think this is indicative of a leak. It may be begin affected by the temperature of the 1 K pot. Isolate IVC and start 1 K pot.
Fill N2 cold trap full.
0105 Temperature of 1 K pot has settled at 1.81 K. Dump pressure 660 mbar: a little low and a little worrying; shall attempt to investigate later.
Open gate valve and condenser line speedivalve. Commence manual condensation procedure through nitrogen cold trap 1.
0130 Mixture left in dump 310 mbar (351 mbar dump pressure in fridge). Valve V12A fully open. Manual condensation procedure complete. Mixing chamber temperature 10.5 K and falling.
0150 Mixing chamber temperature 9.4 K and falling. It's a little warm, but commence manual circulation procedure to see if rate of descent can be increased.
0305 Valve V6 fully open. Manual circulation procedure complete. Mixing chamber temperature 400 mK and falling. Wait for mixing chamber to reach base temperature.
0610 Finally reached a base temperature of 69.5 mK.
0700 Playing around with the 1 K pot needle valve has led to a relatively stable 1 K pot temperature between 1.64 K & 1.65 K. Mixing chamber temperature is 65.4 mK.
1121 Fill N2 cold trap full.