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2013/09/03

0320 Cleaned nitrogen cold trap 2 a couple of times and left it to evacuate for three hours. Pump mixture into dump in preparation for swapping traps.
0435 Closed valves from nitrogen cold trap 2 to He-4 pump, and placed it back in nitrogen bath.
Pressure in dump 687 mbar: appears as though mixture is clean. Close all valves on IGH and nitrogen cold trap 1 speedivalve. Remove nitrogen cold trap 1 from nitrogen bath. Open up line from cold trap 1 to He-4 pump. Allow cold trap 1 to warm to room temperature while being evacuated.
Fill N2 cold trap full. Commence cryocleaning mixture through nitrogen cold trap 2.
0535 Install updates on DAQ computer and restart.
0555 Resume mixing chamber temperature log on DAQ computer.
0620 Cleaned nitrogen cold trap 1 twice. Leave to evacuate.
1020 Closed V11A, V7, V2A and V5A. Put cold trap 1 back in dewar. Refill dewar and play the waiting game (1 hour).
1130 Begin pumping mixture to the dump.
687 mbar in the dump. We want 325 mbar to circulate, so we should leave 362 mbar in the dump. Ambient temperature is at 23.9 C
1230 Begin circulating the mixture.
1310 Increase V12A by 1%.
1450 Fully open valve V12A. Manual condensation procedure complete. Mixture left in dump 362 mbar; therefore mixture in fridge 325 mbar.
1830 We don't seem to be able to get circulation going. Pressures in G1 & G2 at 202 mbar and 184 mbar respectively, and have remained so even when valve V6 completely closed. There is almost certainly a blockage. Pump mixture back into dump by opening valves V5, V6 & V9. Close valve V13A.
2225 Fill N2 cold trap full.
2255 Stop 1 K pot. Switch thermometer. Turn on mixing chamber heater, power 5 mW, to recover mixture at a faster rate.
2335 Increase mixing chamber heater's power to 10 mW.