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2012/05/11

0025 Fill N2 cold trap full.
Close condenser line speedivalve and gate valve. Resume cryocleaning mixture through nitrogen cold trap 2.
1325 Fill N2 cold trap full.
1400 Start 1 K pot.
Pump mixture into dump in preparation for condensation. Start condensing mixture through nitrogen cold trap 1.
1720 Mixture has condensed. Start circulating mixture.
1830 Valve 6 fully open and most of the mixture has been bled from the dump. Let's see what base temperature we achieve…